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Greater insight into the MTDSC technique involving fundamental sinusoidal heat flow equations

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Summary

Modulated temperature DSC was investigated, comparing data found experimentally to that derived from theory. Deviation from theory was found with regard to the amplitude of the modulated heat flow signal when large modulation amplitudes were employed in the experiment. These deviations were determined to be dependent on the absolute temperature and it was concluded that further investigation of the heat flow signal obtained during MTDSC experiments is required.

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Authors and Affiliations

  1. Nanomaterials Research Group, Flinders University, South Australia, 5042, Australia

    I. MacDonald

  2. Nanomaterials Research Group, Flinders University, South Australia, 5042, Australia

    S. Clarke

  3. Nanomaterials Research Group, Flinders University, South Australia, 5042, Australia

    R. Pillar

  4. Nanomaterials Research Group, Flinders University, South Australia, 5042, Australia

    M. Ginic-Markovic

  5. Nanomaterials Research Group, Flinders University, South Australia, 5042, Australia

    J. Matisons

Authors
  1. I. MacDonald
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  2. S. Clarke
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  3. R. Pillar
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  4. M. Ginic-Markovic
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  5. J. Matisons
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MacDonald, I., Clarke, S., Pillar, R. et al. Greater insight into the MTDSC technique involving fundamental sinusoidal heat flow equations. J Therm Anal Calorim 80, 781–786 (2005). https://doi.org/10.1007/s10973-005-0729-z

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  • DOI: https://doi.org/10.1007/s10973-005-0729-z

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