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Synthesis, Spectroscopy, and Magnetic Characterizations of PVP-Assisted Nanoscale Particle

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Abstract

Inverse spinel ferrite of nonmagnetic metal-doped ferro-ferric oxide was synthesized by co-precipitation technique, and its characterizations have been performed by XRD, FTIR, TEM, EDX, VSM, and EPR. XRD figures show the prepared samples in their cubic phase and that their crystallite faces vary from 5.57 to 18.47 nm. FTIR spectra of the as-synthesized samples were performed in the range of 400 and 4000 cm−1 and annealed at 600 ∘C. The TEM revealed that the syllable construction of the nanoscale particles was agglomerated in their crystalline sample. From VSM study, the sample obtained has a doublet pattern, and ferromagnetic performance was observed from the samples. From EPR spectra, the line shape and the g values obtained for the samples conformed to superparamagnetic resonance due to Mg+ 2 ions with a stoichiometric composition. These typical magnetic hypnotic specifications are used for various sensing applications.

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References

  1. Masoudpanah, S.M., Seyyed Ibrahim, S.A., Derakhshani, M., Mirkazemi, S.M.: J. Magn. Magn. Mater. 370, 122–126 (2014). https://doi.org/10.1016/j.jmmm.2014.06.062

    Article  ADS  Google Scholar 

  2. Naseri, M.G., Saion, E.B., Ahangar, H.A., Shaari, A.H., Hashim, M.: Journal of Nanomaterials (2010). https://doi.org/10.1155/2010/907686

    Article  Google Scholar 

  3. Das, H., Sakamoto, N., Aono, H., Shinozakie, K., Suzuki, H., Wakiya, N.: J. Magn. Magn. Mater. 392, 91–100 (2015). https://doi.org/10.1016/j.jmmm.2015.05.029

    Article  ADS  Google Scholar 

  4. Raghasudha, M., Ravinder, D., Veerasomaiah, P.: J. Magn. Magn. Mater. 355, 210–214 (2014). https://doi.org/10.1016/j.jmmm.2013.12.020

    Article  ADS  Google Scholar 

  5. Gadkari, A.B., Shinde, T.J., Vasambekar, P.N.: Mater. Charact. 60(11), 1328–1333 (2009). https://doi.org/10.1016/j.matchar.2009.06.010

    Article  Google Scholar 

  6. Ruan, X., Pei, L., Xuan, S., Yan, Q., Gong, X.: J. Magn. Magn. Mater. 429, 1–10 (2017). https://doi.org/10.1016/j.jmmm.2017.01.003

    Article  ADS  Google Scholar 

  7. Huang, Y.L., Fan, W.B., Hou, Y.H., Guo, K.X., Ouyang, Y.F., Liu, Z.W.: J. Magn. Magn. Mater. 429, 263–269 (2017). https://doi.org/10.1016/j.jmmm.2017.01.043

    Article  ADS  Google Scholar 

  8. Yadav, R.S., Havlica, J., Hnatko, M., Sajgalik, P., Alexander, C., Palou, M., Bartonickova, E., Bohac, M., Frajkorova, F., Masilko, J., Zmrzly, M., Kalina, L., Hajdúchova, M., Enev, V.: J. Magn. Magn. Mater. 378, 190–199 (2015). https://doi.org/10.1016/j.jmmm.2014.11.027

    Article  ADS  Google Scholar 

  9. Prabhakaran, T., Hemalatha, J.: Ceram. Int. 40(2), 3315–3324 (2014). https://doi.org/10.1016/j.ceramint.2013.09.103

    Article  Google Scholar 

  10. Ghasemi, A., Ekhlasi, S., Mousavinia, M.: J. Magn. Magn. Mater. 354, 136–145 (2014). https://doi.org/10.1016/j.jmmm.2013.10.022

    Article  ADS  Google Scholar 

  11. Asghari, M., Ghasemi, A., Paimozd, E., Morisako, A.: Mater. Chem. Phys. 143(1), 161–166 (2013). https://doi.org/10.1016/j.matchemphys.2013.08.045

    Article  Google Scholar 

  12. Khairy, M.: Synth. Met. 189, 34–41 (2014). https://doi.org/10.1016/j.synthmet.2013.12.022

    Article  Google Scholar 

  13. Khanna, L., Verma, N.: J. Magn. Magn. Mater. 336, 1–7 (2013). https://doi.org/10.1016/j.jmmm.2013.02.016

    Article  ADS  Google Scholar 

  14. Nadeem, K., Zeb, F., Azeem Abid, M., Mumtaz, M., Anis Ur Rehman, M.: J. Non-crystalline Solid 400, 45–50 (2014). https://doi.org/10.1016/j.jnoncrysol.2014.05.004

    Article  ADS  Google Scholar 

  15. Hashim, M., Alimuddin, K.S., Shirsath, S.E., Kotnala, R.K., Shah, J., Kumar, R.: Mater. Chem. Phys. 139(2–3), 364–374 (2013). https://doi.org/10.1016/j.matchemphys.2012.09.019

    Article  Google Scholar 

  16. Sagayaraj, R., Aravazhi, S., Praveen, P., Chandrasekaran, G.: J. Mater. Sci. Mater. Electron. 29(3), 2151–2158 (2018). https://doi.org/10.1007/s10854-017-8127-4

    Article  Google Scholar 

  17. Murugesan, C., Okrasa, L., Chandrasekaran, G.: J. Mater. Sci. Mater. Electron. 28(17), 13168–13175 (2017). https://doi.org/10.1007/s10854-017-7152-7

    Article  Google Scholar 

  18. Elilarassi, R., Chandrasekaran, G.: J. Mater. Sci. Mater. Electron. 28(19), 14536–14542 (2017). https://doi.org/10.1007/s10854-017-7317-4

    Article  Google Scholar 

  19. Paul Blessington Selvadurai, A., Pazhanivelu, V., Jagadeeshwaran, C., Murugaraj, R., Mohammed Gazzali, P.M., Chandrasekaran, G.: Appl. Phys. A 123, 13 (2017). https://doi.org/10.1007/s00339-016-0651-1

    Article  ADS  Google Scholar 

  20. Sati, P.C., Kumar, M., Chhoker, S.: J. Ceramics Int. 41(2 part B), 3227–3236 (2015). https://doi.org/10.1016/j.ceramint.2014.11.012

    Article  Google Scholar 

  21. Shafi, K.V.P.M., Koltypin, Y., Gedanken, A.: J. Phys. Chem. B 101(33), 6409–6414 (1997). https://doi.org/10.1021/jp970893q

    Article  Google Scholar 

  22. Naseri, M.G., Saion, E.B., Ahangar, H.A., Hashim, M., Shaari, A.H.: J. Magn. Magn. Mater. 323(13), 1745–1749 (2011). https://doi.org/10.1016/j.jmmm.2011.01.016

    Article  ADS  Google Scholar 

  23. Kasapoglu, N., Birsoz, B., Baykal, A., Koseoglu, Y., Toprak, M.: Formerly Cent. Eur. J. Chem. 5(2) (2007). https://doi.org/10.2478/s11532-007-0005-0

  24. EL-Said Bakeer, D., Abou-Aly, A.I., Mohammed, N.H., Awad, R., Hasebbo, M.: J. Supercond. Nov. Magn. 30(4), 893–902 (2017). https://doi.org/10.1007/s10948-016-3876-5

    Article  Google Scholar 

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Acknowledgements

We remain greatful to the administration of St. Joseph’s College of Arts & Science College (Autonomous), Cuddalore, Tamilnadu, India for providing “Research lab for Nanotechnology and Crystal Growth” laboratory for synthesis of nanomaterials in our work.

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Authors and Affiliations

  1. PG & Research Department of Physics, St. Joseph’s College of Arts and Science (Autonomous), Cuddalore, Tamil Nadu, 607001, India

    R. Sagayaraj

  2. Department of Physics, Arignar Anna Arts College, Villupuram, Tamil Nadu, 605602, India

    S. Aravazhi

  3. Department of Physics, Pondicherry University, Pondicherry, 605014, India

    G. Chandrasekaran

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  1. R. Sagayaraj
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  3. G. Chandrasekaran
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Correspondence to R. Sagayaraj.

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Sagayaraj, R., Aravazhi, S. & Chandrasekaran, G. Synthesis, Spectroscopy, and Magnetic Characterizations of PVP-Assisted Nanoscale Particle. J Supercond Nov Magn 31, 3379–3386 (2018). https://doi.org/10.1007/s10948-018-4593-z

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  • DOI: https://doi.org/10.1007/s10948-018-4593-z

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