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XRD and EXAFS study of nitrato ammine complexes of nitrosyl ruthenium

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Abstract

The structure of trans-[RuNO(NH3)4(H2O)](NO3)3 (I) and trans-[RuNO(NH3)4(NO3)](NO3)2 (II) was determined by XRD. Crystallographic data are as follows: space group I41/a; a = b = 18.280(1) Å, c = 15.129(1) Å, R = 0.0244 (I), and space group Cm, a = 11.5620(3) Å, b = 7.9934(2) Å, c = 7.7864(2) Å, β = 127.124(1)°, R = 0.0139 (II). Interatomic distances for complex particles of fac- and mer- [RuNO(NH3)2(NO3)3] (III and IV, respectively) were determined by EXAFS.

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Authors and Affiliations

  1. A. V. Nikolaev Institute of Inorganic Chemistry, Siberian Division, Russian Academy of Sciences, Novosibirsk, Russia

    E. V. Kabin, V. A. Emel’yanov, I. A. Baidina & T. I. Nedoseykina

  2. Novosibirsk State University, Novosibirsk, Russia

    E. V. Kabin, V. A. Emel’yanov & V. A. Vorob’yov

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  1. E. V. Kabin
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  2. V. A. Emel’yanov
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  3. I. A. Baidina
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  4. T. I. Nedoseykina
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  5. V. A. Vorob’yov
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Correspondence to E. V. Kabin.

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Original Russian Text Copyright © 2010 by E. V. Kabin, V. A. Emel’yanov, I. A. Baidina, T. I. Nedoseykina, and V. A. Vorob’yov

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Translated from Zhurnal Strukturnoi Khimii, Vol. 51, Supplement, pp. S78–S85, 2010.

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Kabin, E.V., Emel’yanov, V.A., Baidina, I.A. et al. XRD and EXAFS study of nitrato ammine complexes of nitrosyl ruthenium. J Struct Chem 51 (Suppl 1), 73–80 (2010). https://doi.org/10.1007/s10947-010-0192-y

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  • DOI: https://doi.org/10.1007/s10947-010-0192-y

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