Skip to main content
Log in

Well-Dispersed Fe3O4/SiO2 Nanoparticles Synthesized by a Mechanical Stirring and Ultrasonication Assisted Stöber Method

  • Published:
Journal of Inorganic and Organometallic Polymers and Materials Aims and scope Submit manuscript

Abstract

Core–shell structured Fe3O4/SiO2 nanoparticles (NPs) sized 40–50 nm with a narrow size distribution have been synthesized by a mechanical stirring and ultrasonication assisted Stöber method at the room temperature. It is shown that the combination of the ultrasonication and mechanical stirring during the preparation process benefits the formation of the well-dispersed NPs. The Fe3O4/SiO2 core–shell microstructure is identified with X-ray diffraction and transmission electron microscopy measurements and such NPs exhibit superparamagnetism.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5

Similar content being viewed by others

References

  1. C.T. Yavuz, J.T. Mayo, W. Yu et al., Science 314, 964 (2006)

    Article  Google Scholar 

  2. Y. Jun, Y. Huh, J. Choi, J. Lee, H. Song et al., J. Am. Chem. Soc. 127, 5732 (2005)

    Article  CAS  Google Scholar 

  3. X.Y. Yang, X.Y. Zhang, Y.F. Ma, Y. Huang et al., J. Mater. Chem. 19, 2710 (2009)

    Article  CAS  Google Scholar 

  4. J. Kim, C. Rong, Y. Lee, J.P. Liu, S. Sun, Chem. Mater. 20, 7242 (2008)

    Article  CAS  Google Scholar 

  5. D. Qi, J. Lu, C. Deng, X. Zhang, J. Phys. Chem. C 113, 15854 (2009)

    Article  CAS  Google Scholar 

  6. Y. Li, X. Xu, D. Qi, C. Deng et al., J. Proteome Res. 7, 2526 (2008)

    Article  CAS  Google Scholar 

  7. J. Wang, S. Zheng, Y. Shao, J. Liu et al., J. Colloid Interface Sci. 349, 293 (2010)

    Article  CAS  Google Scholar 

  8. Z.Z. Xu, C.C. Wang, W.L. Yang, S.K. Fu, J. Mater. Sci. Lett. 40, 4667 (2005)

    CAS  Google Scholar 

  9. W. Stöber, A. Fink, E. Bohn, J. Colloid Interface Sci. 26, 62 (1968)

    Article  Google Scholar 

  10. K.C. Barick, D. Bahadur, Bull. Mater. Sci. 29, 595 (2006)

    Article  CAS  Google Scholar 

  11. Z.L. Lei, Y.L. Li, X.Y. Wei, J. Solid State Chem. 181, 480 (2008)

    Article  CAS  Google Scholar 

  12. C.L. Wang, J.T. Yan, X.J. Cui, H.Y. Wang, J. Colloid Interface Sci. 354, 94 (2011)

    Article  CAS  Google Scholar 

  13. X.J. Sun, F.T. Liu, Q.H. Jiang, Mater. Sci. Forum 688, 364 (2011)

    Article  CAS  Google Scholar 

  14. B. Liu, D.P. Wang, W.H. Huang, M.J. Yu, A.H. Yao, Mater. Res. Bull. 43, 2904 (2008)

    Article  CAS  Google Scholar 

  15. J. Guo, W. Yang, C. Wang, J. He et al., Chem. Mater. 18, 5554 (2006)

    Article  CAS  Google Scholar 

  16. D. Nagao, M. Yokoyama, N. Yamauchi, H. Matsumoto et al., Langmuir 24, 9804 (2008)

    Article  CAS  Google Scholar 

  17. Y.X. Zhang, S.S. Pan, X.M. Teng, Y.Y. Luo et al., J. Phys. Chem. C 112, 9623 (2008)

    Article  CAS  Google Scholar 

  18. Y. Zhang, S.N. Wang, S. Na, J.J. Guan et al., J. Biomed. Mater. Res. A 85A, 840 (2008)

    Article  CAS  Google Scholar 

Download references

Acknowledgments

This work was supported by the Natural Science Foundation of Shandong Province of China (Y2007F44).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Futian Liu.

Additional information

Presented in part at the 1st International Congress on Advanced Materials held in Jinan, PRC, from May 12–17, 2011.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Sun, X., Liu, F., Sun, L. et al. Well-Dispersed Fe3O4/SiO2 Nanoparticles Synthesized by a Mechanical Stirring and Ultrasonication Assisted Stöber Method. J Inorg Organomet Polym 22, 311–315 (2012). https://doi.org/10.1007/s10904-011-9609-0

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10904-011-9609-0

Keywords

Navigation