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One-step hydrothermal synthesis of transition metal oxide electrode material for energy storage applications

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Abstract

Nanostructured CuO/ZnO composite has been prepared by hydrothermal method. The prepared nanocomposite has been investigated by various characterization techniques such as PXRD, FTIR, SEM with EDAX, UV and electrochemical workstation. Structural analysis shows the arrangement of CuO/ZnO, composition of monoclinic CuO with space group of C2/c, and hexagonal ZnO with space group of P63mc. The nanorods like morphology of the nanocomposite have been confirmed by SEM analysis. Optical bandgap of the material has been calculated by Tauc’s plot and obtained bandgap values are 2.83 eV and 2.68 eV, respectively. In GCD analysis, maximum specific capacitance is observed in modified working electrode at scan rate of 1 mA, which continues remarkable cycling stability within the retention ratio of 40.86% after 1000 cycles.

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Acknowledgements

The authors are grateful to the management, Kalasalingam Academy of Research and Education, Krishnankoil, India for their support.

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Authors and Affiliations

  1. Department of Physics, School of Advanced Sciences, Kalasalingam Academy of Research and Education, Krishnankoil, 626 126, India

    Vadivel Siva, Anbazhagan Murugan, Abdul samad Shameem & Sultan Asath Bahadur

  2. Condensed Matter Physics Laboratory, International Research Centre, Kalasalingam Academy of Research and Education, Krishnankoil, 626 126, India

    Vadivel Siva, Anbazhagan Murugan, Abdul samad Shameem & Sultan Asath Bahadur

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  1. Vadivel Siva
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  2. Anbazhagan Murugan
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Correspondence to Sultan Asath Bahadur.

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Siva, V., Murugan, A., Shameem, A.s. et al. One-step hydrothermal synthesis of transition metal oxide electrode material for energy storage applications. J Mater Sci: Mater Electron 31, 20472–20484 (2020). https://doi.org/10.1007/s10854-020-04566-2

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