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Facile synthesis and characterization of CdTiO3 nanoparticles by Pechini sol–gel method

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Abstract

In this work, CdTiO3 nanoparticles were synthesized through reaction between Cd(CH3COO)2.2H2O, Ti(OC4H9)4, trimesic acid as a new chelating agent and ethanol as solvent by Pechini sol–gel method. X-ray diffraction (XRD) patterns showed that CdTiO3 nanostructures have rhombohedral structure with diameter of about 35.61 nm. The structure, morphology and size of CdTiO3 nanoparticles were characterized by FT-IR, XRD, SEM and EDAX. The optical properties of the products were studied by DRS. Based on the results of experiments, it was found that temperature and time of calcination, pH and the solvent of reaction are important parameters for formation of CdTiO3 nanoparticles. Utilizing trimesic acid (benzene-1,3,5-tricarboxylic acid) as a new chelating agent for preparation of CdTiO3 nanostructures was initiative of this work.

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References

  1. O. Yamamoto, Y. Takeda, R. Kanno, M. Noda, Solid State Ionics 22, 241 (1987)

    Article  Google Scholar 

  2. H. Obayashi, Y. Sakurai, T. Gejo, J. Solid State Chem. 17, 299 (1976)

    Article  Google Scholar 

  3. Y. Shimizu, K. Uemura, N. Miura, N. Yamazoe, Chem. Lett., 17, 1979 (1988)

    Article  Google Scholar 

  4. M. Skoglundh, L. Lowedalh, K. Janson, L. Dahl, M. Nygren, Appl. Catal. 53, 56 (1970)

    Google Scholar 

  5. A. Montenero, M. Canali, G. Gnappi, D. Bersani, P.P. Lottici, P. Nunziante et al., Appl. Organomet. Chem. 11, 137 (1997)

    Article  Google Scholar 

  6. X. Zhang, H. Wang, A. Huang, H. Xu, Y. Zhang, D. Yu et al., J. Mater. Sci. 38, 2353 (2003)

    Article  Google Scholar 

  7. T. Bein, K. Brown, G.C. Fye, J. Am. Ceram. Soc. 111, 7640 (1989)

    Google Scholar 

  8. G.L. Catchen, S.J. Wukitch, D.M. Spaar, Phys. Rev. B 42, 1885 (1990)

    Article  Google Scholar 

  9. YJ. Shan, H. Mori, H. Imoto, Ferroelectronics 270, 381 (2002)

    Article  Google Scholar 

  10. O.E. Fesenko, V.V. Eremkin, V.G. Smotrakov, Sov. Phys Solid State 28, 511 (1986)

    Google Scholar 

  11. A.R. Phani, M. Passacantando, S. Santucci, J. Mater. Sci. 35, 5295 (2000)

    Article  Google Scholar 

  12. A.R. Phani, S. Santucci, J. Phys. 18, 6965 (2006)

    Google Scholar 

  13. S.A. Maye´n-Herna´ndez, J. Santos-Cruz, G. Torres-Delgado, R. Castanedo-Pe´rez, J. Ma´rquez-Marı´n, J.G. Mendoza-Alvarez et al, Surf. Coat. Technol. 200, 3567 (2006)

    Article  Google Scholar 

  14. S.A. Maye´n-Herna´ndez, G. Torres-Delgado, R. Castanedo-Pe´rez, A. Cruz-Orea, J. G. Mendoza-Alvarez and O. Zelaya-Angel, Sol. Energy Mater. Sol. Cells 90, 2280 (2006)

    Article  Google Scholar 

  15. X.M. Liu, G. Yang, S.Y. Fu, Mater. Sci. Eng. C 27, 750 (2007)

    Article  Google Scholar 

  16. P.K. Sharma, M.H. Jilavi, V.K. Varadan, H. Schmidt, J. Phys. Chem. Solids 63, 171 (2002)

    Article  Google Scholar 

  17. W.G. Klemperer, S.D. Ramamurthy, in: C.J. Brinker, D.E. Clarke, D.E. Ulrich, Material Research Society Symposium Proceedings, vol. 121, Pittsburgh, PA, 1 (1988)

  18. S.A. Mayén-Hernández, J. Santos-Cruz, G. Torres-Delgado, R. Castanedo- Pérez, J. Márquez-Marín, J.G. Mendoza-Alvarez, O. Zelaya-Angel, Surf. Coat. Technol. 200, 3567 (2006)

    Article  Google Scholar 

  19. S.A. Mayen-Hernandez, G. Torres-Delgado, R. Castanedo-Perez, H. Cruz-Orea, J.G. Mendoza-Alvarez, O. Zelaya-Angel, Sol. Energy Mater. Sol Cells 90, 2280 (2006)

    Article  Google Scholar 

  20. S.A. Mayen-Hernandez, G. Torres-Delgado, R. Castanedo-Perez, J.G. Mendoza-Alvarez, O. Zelaya-Angel, Mater. Chem. Phys. 115, 530 (2009)

    Article  Google Scholar 

  21. M.E. de Anda Reyes, G. Torres Delgado, R. Castanedo Perez, J. Marquez Marin, O. Zelaya Angel, J. Photochem. Photobiol. A 228, 22 (2012)

    Article  Google Scholar 

  22. D.L. Liao, C.A. Badour, B.Q. Liao, J. Photochem. Photobiol. A 194, 11 (2008)

    Article  Google Scholar 

  23. M. Goudarzi, D. Ghanbari, M. Salavati-Niasari, J. Nanostruct. 5, 105–110 (2015)

    Google Scholar 

  24. A. Esmaeili-Bafghi-Karimabad, D. Ghanbari, M. Salavati-Niasari, H. Safardoust-Hojaghan, J. Nanostruct. 5, 263–269 (2015)

    Google Scholar 

  25. S. Moshtaghi, M. Salavati-Niasari, D. Ghanbari. J. Nanostruct. 5, 169–174 (2015)

    Article  Google Scholar 

  26. F. Beshkar, M. Salavati-Niasari, J. Nanostruct. 5, 17–23 (2015)

    Article  Google Scholar 

  27. M. Mousavi-Kamazani, M. Salavati-Niasari, D. Ghanbari, J. Nanostruct. 2, 363–368 (2012)

    Google Scholar 

  28. Y.Q. Li, J.L. Wang, S.Y. Fu, S.G. Mei, J.M. Zhang, K. Yong, Mater. Res. Bull. 45, 677 (2010)

    Article  Google Scholar 

  29. Y.Q. Li, K. Yong, H.M. Xiao, W.J. Ma, G.L. Zhang, S.Y. Fu, Mater. Lett. 64, 1735 (2010)

    Article  Google Scholar 

  30. P.K. Sharma, V.V. Varadan, V.K. Varadan, J. Eur. Ceram. Soc 23, 659 (2003)

    Article  Google Scholar 

Download references

Acknowledgements

The authors are grateful to the council of Iran National Science Foundation (INSF) and University of Kashan for supporting this work by Grant No (159271/51579).

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Authors and Affiliations

  1. Institute of Nano Science and Nano Technology, University of Kashan, Kashan, P.O. Box 87317-51167, Iran

    Masoud Salavati-Niasari, Ali Sobhani-Nasab, Maryam Shakouri-Arani & Masood Hamadanian

  2. Young Researchers and Elite Club, Bandar Abbas Branch, Islamic Azad University, Bandar Abbas, Iran

    Faezeh Soofivand

  3. Center for Research in Nanotechnology & Catalysis (NANOCAT), Institute of Postgraduate Studies (IPS) Building, University of Malaya, 3rd Floor, Block A, Kuala Lumpur, 50603, Malaysia

    Samira Bagheri

Authors
  1. Masoud Salavati-Niasari
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  2. Faezeh Soofivand
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  3. Ali Sobhani-Nasab
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  4. Maryam Shakouri-Arani
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  5. Masood Hamadanian
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Correspondence to Masoud Salavati-Niasari.

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Salavati-Niasari, M., Soofivand, F., Sobhani-Nasab, A. et al. Facile synthesis and characterization of CdTiO3 nanoparticles by Pechini sol–gel method. J Mater Sci: Mater Electron 28, 14965–14973 (2017). https://doi.org/10.1007/s10854-017-7369-5

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  • DOI: https://doi.org/10.1007/s10854-017-7369-5

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