Skip to main content
Log in

Effect of energy density on the interface evolution of stainless steel 316L deposited upon INC 625 via directed energy deposition

  • Metals & corrosion
  • Published:
Journal of Materials Science Aims and scope Submit manuscript

Abstract

Directed energy deposition (DED) is an additive manufacturing technique that permits the manufacturing of complex multi-material components. In the present study, DED was used for the fabrication of Inconel 625 and stainless steel 316L couples. The effect of input energy density on the evolution of the dissimilar metal interface and its mechanical properties was explored by varying the laser power for each build. Columns that transitioned directly from Inconel 625 to stainless steel 316L were deposited onto mild steel substrates. The columns were cross-sectioned and characterised by coupling physical characterisation with microhardness. Scanning electron microscopy and compositional mapping were used to correlate the relationship between energy density and the produced functional gradient. It was seen that high energy deposition resulted in a measurable, remelted layer solute (RLS) fraction that comprised each deposited layer, creating a stepwise-graded interface. The RLS fraction was consistent across each layer of the interface and was influenced by the energy density of the build. Changes in the RLS affected the length of the graded interface but did not have a significant influence the mechanical properties. The yield strength and ultimate tensile strength of the through-interface compared well with the traditional wrought stainless steel 316L but suffered in ductility. Mix-mode fracture tended to occur in the near stainless steel composition regions.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Figure 1
Figure 2
Figure 3
Figure 4
Figure 5
Figure 6
Figure 7
Figure 8
Figure 9
Figure 10
Figure 11

Similar content being viewed by others

References

  1. Lundin CD (1982) Dissimilar metal welds-transition joints literature review, Weld Res Suppl. https://files.aws.org/wj/supplement/WJ_1982_02_s58.pdf.

  2. Sun Z, Ion JC (1995) Laser welding of dissimilar metal combinations. J Mater Sci 30:4205–4214. https://doi.org/10.1007/BF00361499

    Article  CAS  Google Scholar 

  3. Messler RW (1999) Principles of welding, Wiley. New York. https://doi.org/10.1002/9783527617487

    Article  Google Scholar 

  4. Ramakrishnan P (1972) Welding metallurgy, Wiley. New York. https://doi.org/10.22486/iwj.v4i3.150243

    Article  Google Scholar 

  5. Cai W, Daehn G, Vivek A, Li J, Khan H, Mishra RS, Komarasamy M (2019) A state-of-the-art review on solid-state metal joining. J. Manuf. Sci. Eng. Trans. ASME. https://doi.org/10.1115/1.4041182

    Article  Google Scholar 

  6. Shamsaei N, Yadollahi A, Bian L, Thompson SM (2015) An overview of direct laser deposition for additive manufacturing; Part II: mechanical behavior, process parameter optimization and control. Addit Manuf 8:12–35. https://doi.org/10.1016/j.addma.2015.07.002

    Article  Google Scholar 

  7. Liu W, DuPont JN (2003) Fabrication of functionally graded TiC/Ti composites by laser engineered net shaping. Scr Mater 48:1337–1342. https://doi.org/10.1016/S1359-6462(03)00020-4

    Article  CAS  Google Scholar 

  8. Mahamood RM, Akinlabi ET (2015) Laser metal deposition of functionally graded Ti6Al4V/TiC. Mater Des 84:402–410. https://doi.org/10.1016/j.matdes.2015.06.135

    Article  CAS  Google Scholar 

  9. Wang F, Mei J, Wu X (2006) Microstructure study of direct laser fabricated Ti alloys using powder and wire. Appl Surf Sci 253:1424–1430. https://doi.org/10.1016/j.apsusc.2006.02.028

    Article  CAS  Google Scholar 

  10. Li W, Liou F, Newkirk J, Brown Taminger KM, Seufzer WJ (2017) Investigation on Ti6Al4V-V-Cr-Fe-SS316 multi-layers metallic structure fabricated by laser 3D printing. Sci Rep 7:1–14. https://doi.org/10.1038/s41598-017-08580-z

    Article  CAS  Google Scholar 

  11. Li W, Yan L, Karnati S, Liou F, Newkirk J, Taminger KMB, Seufzer WJ (2017) Ti-Fe intermetallics analysis and control in joining titanium alloy and stainless steel by laser metal deposition. J Mater Process Technol 242:39–48. https://doi.org/10.1016/j.jmatprotec.2016.11.010

    Article  CAS  Google Scholar 

  12. Farren JD, DuPont JN, Noecker FF (2007) Fabrication of a carbon steel-to-stainless steel transition joint using direct laser deposition—a feasibility study. Weld J 86:55–61

    Google Scholar 

  13. Shah K, ul Haq I, Khan A, Shah SA, Khan M, Pinkerton AJ (2014) Parametric study of development of Inconel-steel functionally graded materials by laser direct metal deposition. Mater Des 54:531–538. https://doi.org/10.1016/j.matdes.2013.08.079

    Article  CAS  Google Scholar 

  14. Carroll BE, Otis RA, Borgonia JP, Suh JO, Dillon RP, Shapiro AA, Hofmann DC, Liu ZK, Beese AM (2016) Functionally graded material of 304L stainless steel and inconel 625 fabricated by directed energy deposition: characterization and thermodynamic modeling. Acta Mater 108:46–54. https://doi.org/10.1016/j.actamat.2016.02.019

    Article  CAS  Google Scholar 

  15. Chen B, Su Y, Xie Z, Tan C, Feng J (2020) Development and characterization of 316L/Inconel625 functionally graded material fabricated by laser direct metal deposition. Opt Laser Technol 123:105916. https://doi.org/10.1016/j.optlastec.2019.105916

    Article  CAS  Google Scholar 

  16. Belloni G, Caironi G, Gariboldi A, Lo Conte A, Bovisa C (2001) Effect of microstructural alteration on the creep behaviour and effect of flaws in 50cr50ni-nb engineering alloy. In: SMiRT 16, pp 1–8

  17. Naffakh H, Shamanian M, Ashrafizadeh F (2009) Dissimilar welding of AISI 310 austenitic stainless steel to nickel-based alloy Inconel 657. J Mater Process Technol 209:3628–3639. https://doi.org/10.1016/j.jmatprotec.2008.08.019

    Article  CAS  Google Scholar 

  18. Agilan M, Krishna SC, Manwatkar SK, Eg V, Sivakumar D, Pant B (2012) Effect of welding processes (GTAW & EBW) and solutionizing temperature on microfissuring tendency in inconel 718 welds. Mater Sci Forum 710:603–607. https://doi.org/10.4028/www.scientific.net/MSF.710.603

    Article  CAS  Google Scholar 

  19. Caironi G, Gariboldi E, Silva G, Vedani M (1994) Influence of preliminary heat treatments on microstructure, mechanical properties and creep behaviour of a 50Cr-50Ni niobium containing alloy. Mater Sci Forum 163–6:181–188. https://doi.org/10.4028/www.scientific.net/msf.163-165.181

    Article  Google Scholar 

  20. Devendranath Ramkumar K, Patel SD, Sri Praveen S, Choudhury DJ, Prabaharan P, Arivazhagan N, Xavior MA (2014) Influence of filler metals and welding techniques on the structure-property relationships of Inconel 718 and AISI 316L dissimilar weldments. Mater Des 62:175–188. https://doi.org/10.1016/j.matdes.2014.05.019

    Article  CAS  Google Scholar 

  21. Bansal A, Sharma AK, Das S, Kumar P (2016) On microstructure and strength properties of microwave welded Inconel 718/ stainless steel (SS-316L). In: Proc. Inst. Mech. Eng. Part L J. Mater. Des. Appl. pp 939–948. https://doi.org/10.1177/1464420715589206

  22. Lin CM (2013) Relationships between microstructures and properties of buffer layer with Inconel 52M clad on AISI 316L stainless steel by GTAW processing. Surf Coatings Technol 228:234–241. https://doi.org/10.1016/j.surfcoat.2013.04.035

    Article  CAS  Google Scholar 

  23. Ramkumar T, Selvakumar M, Narayanasamy P, Begam AA, Mathavan P, Raj AA (2017) Studies on the structural property, mechanical relationships and corrosion behaviour of Inconel 718 and SS 316L dissimilar joints by TIG welding without using activated flux. J Manuf Process 30:290–298. https://doi.org/10.1016/j.jmapro.2017.09.028

    Article  Google Scholar 

  24. Griffith ML, Harwell LD, Romero JT, Schlienger E, Atwood CL, Smugeresky JE (1997) Multi-material processing by LENSTM, Proc. 8th Solid Free. Fabr. Symp. 387–394

  25. ASM International (2018) Gray iron In: Met. Handb. Desk Ed., ASM International, Materials Park, OH, pp 309–314. https://doi.org/10.31399/asm.hb.mhde2.a0003107

  26. Zhang K, Liu W, Shang X (2007) Research on the processing experiments of laser metal deposition shaping. Opt Laser Technol 39:549–557. https://doi.org/10.1016/j.optlastec.2005.10.009

    Article  CAS  Google Scholar 

  27. Ocylok S, Alexeev E, Mann S, Weisheit A, Wissenbach K, Kelbassa I (2014) Correlations of melt pool geometry and process parameters during laser metal deposition by coaxial process monitoring. Phys Procedia 56:228–238. https://doi.org/10.1016/j.phpro.2014.08.167

    Article  Google Scholar 

  28. Hofman JT, De Lange DF, Pathiraj B, Meijer J (2011) FEM modeling and experimental verification for dilution control in laser cladding. J Mater Process Technol 211:187–196. https://doi.org/10.1016/j.jmatprotec.2010.09.007

    Article  Google Scholar 

  29. ASM International. Handbook Committee, ASM Handbook, Volume 15, 9th Editio, ASM International, 2008. https://doi.org/10.31399/asm.hb.v15.9781627081870

  30. Yadollahi A, Shamsaei N, Thompson SM, Seely DW (2015) Effects of process time interval and heat treatment on the mechanical and microstructural properties of direct laser deposited 316L stainless steel. Mater Sci Eng A 644:171–183. https://doi.org/10.1016/j.msea.2015.07.056

    Article  CAS  Google Scholar 

  31. Guo P, Zou B, Huang C, Gao H (2017) Study on microstructure, mechanical properties and machinability of efficiently additive manufactured AISI 316L stainless steel by high-power direct laser deposition. J Mater Process Technol 240:12–22. https://doi.org/10.1016/j.jmatprotec.2016.09.005

    Article  CAS  Google Scholar 

  32. Zheng B, Zhou Y, Smugeresky JE, Schoenung JM, Lavernia EJ (2008) Thermal behavior and microstructure evolution during laser deposition with laser-engineered net shaping: Part II. Experimental investigation and discussion. Metall Mater Trans A Phys Metall Mater Sci 39:2237–2245. https://doi.org/10.1007/s11661-008-9566-6

    Article  CAS  Google Scholar 

  33. Zhang X, Chen Y, Liou F (2019) Fabrication of SS316L-IN625 functionally graded materials by powder-fed directed energy deposition. Sci Technol Weld Join 24:504–516. https://doi.org/10.1080/13621718.2019.1589086

    Article  CAS  Google Scholar 

  34. Khayat ZR, Palmer TA (2018) Impact of iron composition on the properties of an additively manufactured solid solution strengthened nickel base alloy. Pa State Univ. https://doi.org/10.1016/j.msea.2018.01.112

    Article  Google Scholar 

  35. DuPont JN, Robino CV, Michael JR, Nous MR, Marder AR (1998) Solidification of Nb-bearing superalloys: Part I. Reaction sequences. Metall Mater Trans A Phys Metall Mater Sci 29:2785–2796. https://doi.org/10.1007/s11661-998-0319-3

    Article  Google Scholar 

  36. Murr LE, Martinez E, Gaytan SM, Ramirez DA, MacHado BI, Shindo PW, Martinez JL, Medina F, Wooten J, Ciscel D, Ackelid U, Wicker RB (2011) Microstructural architecture, microstructures, and mechanical properties for a nickel-base superalloy fabricated by electron beam melting. Metall Mater Trans A Phys Metall Mater Sci 42:3491–3508. https://doi.org/10.1007/s11661-011-0748-2

    Article  CAS  Google Scholar 

  37. Cieslak M (1991) The welding and solidification metallurgy of alloy 625. Weld J 70:49

    Google Scholar 

  38. Zhang D, Qiu D, Gibson MA, Zheng Y, Fraser HL, StJohn DH, Easton MA (2019) Additive manufacturing of ultrafine-grained high-strength titanium alloys. Nature 576:91–95. https://doi.org/10.1038/s41586-019-1783-1

    Article  CAS  Google Scholar 

  39. Collins PC, Brice DA, Samimi P, Ghamarian I, Fraser HL (2016) Microstructural control of additively manufactured metallic materials. Annu Rev Mater Res 46:63–91. https://doi.org/10.1146/annurev-matsci-070115-031816

    Article  CAS  Google Scholar 

  40. Bontha S, Klingbeil NW, Kobryn PA, Fraser HL (2009) Effects of process variables and size-scale on solidification microstructure in beam-based fabrication of bulky 3D structures. Mater Sci Eng A 513–514:311–318. https://doi.org/10.1016/j.msea.2009.02.019

    Article  CAS  Google Scholar 

Download references

Acknowledgements

We gratefully acknowledge the support of the Monash Centre for Electron Microscopy (MCEM), the Monash Centre for Additive Manufacturing (MCAM) and Woodside Energy.

Author information

Authors and Affiliations

Authors

Contributions

DF was involved in conceptualisation, methodology, formal analysis, investigation writing–original draft preparation, writing—review & editing. AM was involved in conceptualisation, review & editing and supervision. NB was involved in conceptualisation, methodology, writing—review & editing, supervision, project administration and funding acquisition.

Corresponding author

Correspondence to D. R. Feenstra.

Ethics declarations

Conflict of interest

The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Feenstra, D.R., Molotnikov, A. & Birbilis, N. Effect of energy density on the interface evolution of stainless steel 316L deposited upon INC 625 via directed energy deposition. J Mater Sci 55, 13314–13328 (2020). https://doi.org/10.1007/s10853-020-04913-y

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10853-020-04913-y

Navigation