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Preparation and characterization of magnetic carbon nanomaterials bearing APTS–silica on their surface

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Abstract

The formation of metal-encapsulated carbon nanomaterials by using metallic catalysts (iron, cobalt, and nickel) has been studied. Moreover, these materials were coated with silica surface modified by (3-Aminopropyl)-trimethoxysilane (APTS). Each intermediate structure was confirmed by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The surface morphology of silica-coated carbon nanomaterials was analyzed by scanning electron microscopy (SEM). The modified, APTS–silica surface was additionally characterized by Fourier transform infrared spectroscopy (FT-IR), elemental (EA), and thermogravimetric analysis (TGA).

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Acknowledgements

The authors are grateful to Dr. E. Borowiak-Paleń (Institute of Chemical and Environmental Engineering, West Pomeranian University of Technology, Szczecin) for the HRTEM images of iron sample after ethylene decomposition.

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Authors and Affiliations

  1. Institute of Chemical and Environment Engineering, West Pomeranian University of Technology, Pułaskiego 10, 70-322, Szczecin, Poland

    Urszula Narkiewicz, Iwona Pełech & Marcin Podsiadły

  2. Faculty of Chemistry, Adam Mickiewicz University, Grunwaldzka 6, 60-780, Poznan, Poland

    Michał Cegłowski, Grzegorz Schroeder & Joanna Kurczewska

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  1. Urszula Narkiewicz
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  2. Iwona Pełech
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  3. Marcin Podsiadły
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  4. Michał Cegłowski
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  5. Grzegorz Schroeder
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  6. Joanna Kurczewska
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Correspondence to Joanna Kurczewska.

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Narkiewicz, U., Pełech, I., Podsiadły, M. et al. Preparation and characterization of magnetic carbon nanomaterials bearing APTS–silica on their surface. J Mater Sci 45, 1100–1106 (2010). https://doi.org/10.1007/s10853-009-4052-0

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