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Physico-chemical and anatomical characterization of residual lignocellulosic fibers

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Abstract

Anatomical and physico-chemical properties of residual natural fibers (sugarcane bagasse, coconut fibers and peanut hulls) were characterized in order to evaluate their potential for use in the production of particleboard. The bulk density was determined by helium pycnometer and the chemical characteristics by using an electronic pH meter (for pH determination) on fibers dissolved in acidic and neutral detergents (to determine the levels of cellulose, hemicellulose and lignin). The anatomical characteristics were established using scanning electron microscopy coupled with an X-ray detector system, as well as energy dispersive X-ray spectroscopy. Results indicated similarities and differences between physico-chemical and anatomical characteristics of the residual lignocellulosic fibers when compared with the Pinus sp. wood commercially employed in particleboard production. Bulk density and pH for residual lignocellulosic fibers and Pinus sp. wood presented analogous values. Similar amounts of cellulose and lignin were identified between waste fibers and Pinus sp. wood. The presence of silica was identified in coconut fiber, peanut hull and sugarcane bagasse waste fibers, and may affect the mechanical characteristics of panels. Coconut and sugarcane bagasse fibers show surface pores with diameters ranging from 1.2 to 2.1 μm, below the 5 μm identified for Pinus sp. wood. Both fibers present pores distributed over their entire surface, whereas peanut hull fibers have no pores on their surface. This characteristic contributes to resin dispersion among particles, reflecting positively on the physical–mechanical properties of the panels. Particleboards produced with residual lignocellulosic fibers present similar physical–mechanical properties to those of Pinus sp. wood panels.

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Acknowledgments

Research Foundation of the São Paulo State—FAPESP; National Council for Scientific and Technological Development—CNPq; Financier of Studies and Projects—FINEP and Coordination of Improvement of Higher Education Personnel—CAPES.

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Correspondence to Juliano Fiorelli.

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Fiorelli, J., Gomide, C.A., Lahr, F.A.R. et al. Physico-chemical and anatomical characterization of residual lignocellulosic fibers. Cellulose 21, 3269–3277 (2014). https://doi.org/10.1007/s10570-014-0398-9

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