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Synthesis of (chloromethyl)dimethylsilanol

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Abstract

(Chloromethyl)dimethylsilanol was synthesized by the hydrolysis of (chloromethyl)dimethylchlorosilane, N-[(chloromethyl)dimethylsilyl]amines, or N-(chloromethyl)dimethylsilyl-N-methylamide of diisopropylphosphoric acid.

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References

  1. Noll W (1968) Chemistry and technology of silicones. Academic Press, New York

    Google Scholar 

  2. Lickiss PD (1995) Adv Inorg Chem 42:147

    Article  CAS  Google Scholar 

  3. Murugavel R, Voigt A, Walawalkar MG, Roesky HW (1996) Chem Rev 96:2205

    Article  CAS  Google Scholar 

  4. Murugavel R, Chandrasekhar V, Roesky HW (1996) Acc Chem Res 29:183

    Article  CAS  Google Scholar 

  5. Chandrasekhar V, Boomishankar R, Nagendran S (2004) Chem Rev 104:5847

    Article  CAS  Google Scholar 

  6. Iler RK (1979) The Chemistry of silica: solubility polymerization colloid and surface properties and biochemistry of silica. Wiley and Sons, New York

    Google Scholar 

  7. Ehrlich H, Demadis KD, Pokrovsky OS, Koutsoukos PG (2010) Chem Rev 110:4656

    Article  CAS  Google Scholar 

  8. Coradin T, Livage J (2007) Acc Chem Res 40:819

    Article  CAS  Google Scholar 

  9. Perry CC (2003) Rev Mineral Geochem 54:291

    Article  CAS  Google Scholar 

  10. Hirabayashi K, Nishihara Y, Mori A, Hiyama T (1998) Tetrahedron Lett 39:7893

    Article  CAS  Google Scholar 

  11. Hirabayashi K, Kawashima J, Nishihara Y, Mori A, Hiyama T (1999) Org Lett 1:299

    Article  CAS  Google Scholar 

  12. Hirabayashi K, Kondo T, Toriyama F, Nishihara Y, Mori A (2000) Bull Chem Soc Jpn 73:749

    Article  CAS  Google Scholar 

  13. Denmark SE, Wehrli D (2000) Org Lett 2:565

    Article  CAS  Google Scholar 

  14. Hirabayashi K, Mori A, Kawashima J, Suguro M, Nishihara Y, Hiyama T (2000) J Org Chem 65:5342

    Article  CAS  Google Scholar 

  15. Colvin EW (1998) Silicon reagents in organic synthesis. Academic Press, London

    Google Scholar 

  16. Drake R, MacKinnon I, Taylor R (1998) In: Rappoport Z, Apeloig Y (eds) The chemistry of organic silicon compounds. Wiley, New York

    Google Scholar 

  17. Tacke R, Linoh H (1989) In: Patai S, Rappoport Z (eds) The chemistry of organic silicon compounds. Wiley, New York

    Google Scholar 

  18. Sieburth SM, Nittoli T, Mutahi AM, Guo L (1998) Angew Chem Int Ed 37:812

    Article  CAS  Google Scholar 

  19. Kim J, Glekasa A, Sieburth SM (2000) Bioorg Med Chem Lett 12:3625

    Article  Google Scholar 

  20. Sieburth SM, Chen CA (2006) Eur J Org Chem 2:311

    Article  Google Scholar 

  21. Catlow CRA (ed) (1992) Modelling of structure and reactivity in zeolites. Academic Press, London

    Google Scholar 

  22. Bilda S, Röhr G, Lange D, Popowski E, Kelling H (1988) Z Anorg Allg Chem 564:155

    Article  CAS  Google Scholar 

  23. Bilda S, Lange D, Popowski E, Kelling HS, Bilda D, Lange E, Popowski H, Kelling (1987) Z Anorg Allg Chem 550:186

    Article  CAS  Google Scholar 

  24. Wieber M, Schmidt M (1962) Angew Chem Int Ed 1:661

    Article  Google Scholar 

  25. Wieber M, Schmidt M (1963) Chem Ber 96:1016

    Article  CAS  Google Scholar 

  26. Voss P, Elsner A, Popowski E, Schott G, Kelling H (1978) Z Anorg Allg Chem 445:219

    Article  CAS  Google Scholar 

  27. Ishimoto R, Kamata K, Mizuno N (2009) Angew Chem Int Ed 48:8900

    Article  CAS  Google Scholar 

  28. Cella JA, Carpenter JC (1994) J Organomet Chem 480:23

    Article  CAS  Google Scholar 

  29. Suslova EN, Shainyan BA (2011) Russ J Gen Chem 81:1735

    Article  CAS  Google Scholar 

  30. Baruah JB (2007) In: Clarson SJ, Fitzgerald JJ, Owen MJ, Smith SD, Van Dyke ME (eds) ACS symposium series, vol 964. American Chemical Society, Washington, p 69

    Google Scholar 

  31. Deka K, Sarma RJ, Baruah JB (2005) Inorg Chem Commun 8:1082

    Article  CAS  Google Scholar 

  32. Kabachnik MI (1979) Usp Khimii 48:1523

    Google Scholar 

  33. Grobe J, Heyer G (1973) J Organomet Chem 61:133

    Article  CAS  Google Scholar 

  34. Eisch JJ, Chiu CS (1994) Heteroatom Chem 5:265

    Article  CAS  Google Scholar 

  35. Lazareva NF, Doronina EP, Belogolova EF, Shainyan BA, Sidorkin VF (2007) Russ J Gen Chem 77:1177

    Article  CAS  Google Scholar 

  36. Gordon A, Ford R (1972) The Chemist’s companion. A handbook of practical data techniques and references. John Wiley & Sons, New York

    Google Scholar 

Download references

Acknowledgments

This work was performed with the financial support from the Russian Foundation for Basic Research (Grant No: 14-03-31462).

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Authors and Affiliations

  1. Irkutsk Institute of Chemistry A. E. Favorsky, Siberian Branch of the Russian Academy of Sciences, Favorsky st., 1, 664033, Irkutsk, Russian Federation

    Nataliya F. Lazareva & Alexey Yu Nikonov

Authors
  1. Nataliya F. Lazareva
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  2. Alexey Yu Nikonov
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Correspondence to Nataliya F. Lazareva.

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Lazareva, N.F., Nikonov, A.Y. Synthesis of (chloromethyl)dimethylsilanol. Monatsh Chem 146, 983–986 (2015). https://doi.org/10.1007/s00706-014-1366-7

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  • DOI: https://doi.org/10.1007/s00706-014-1366-7

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