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Convenient and High-Yielding Preparations of Mono(5-carboxy-2-ethylpentyl) Phthalate and its Ring-Deuterated Isomer – The “Third” Major Metabolite of Bis(2-ethylhexyl) Phthalate

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Summary.

The synthesis of an oxidative major metabolite of bis(2-ethylhexyl) phthalate is described. The target molecule and its ring-deuterated isomer were obtained via acylation of the appropriate ω-hydroxy benzyl ester or the corresponding carboxylate with phthalic anhydride or phthalic anhydride-d4. All transformation steps proceed with high yields.

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Authors and Affiliations

  1. Institut für Dünnschichttechnologie und Mikrosensorik e.V., D-14513, Teltow, Germany

    Hans-Detlev Gilsing & Dietrich Prescher

  2. Institut und Poliklinik für Arbeits-, Sozial- und Umweltmedizin der Universität Erlangen-Nürnberg, D-91054, Erlangen, Germany

    Jürgen Angerer

Authors
  1. Hans-Detlev Gilsing
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  2. Jürgen Angerer
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  3. Dietrich Prescher
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Correspondence to Hans-Detlev Gilsing.

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Gilsing, HD., Angerer, J. & Prescher, D. Convenient and High-Yielding Preparations of Mono(5-carboxy-2-ethylpentyl) Phthalate and its Ring-Deuterated Isomer – The “Third” Major Metabolite of Bis(2-ethylhexyl) Phthalate. Monatshefte für Chemie 136, 795–801 (2005). https://doi.org/10.1007/s00706-004-0267-6

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  • DOI: https://doi.org/10.1007/s00706-004-0267-6

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