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Iron oxide/MCM-41 mesoporous nanocomposites and their magnetorheology

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Abstract

Mesoporous nanocomposite materials of magnetic iron oxide-containing MCM-41 (IO/MCM-41) were prepared by simple thermal oxidation of Fe-containing MCM-41 initially prepared by a direct synthesis route using Fe3+ salt. The magnetic saturation of the fabricated nanocomposite materials was measured using a vibrating sample magnetometer, while surface morphology and inner framework of the composite materials were studied using a field emission scanning electron microscope and a transmission electron microscope to confirm their mesoporous nanocomposite formation. The fabricated magnetic materials were then adopted as a magnetorheological (MR) fluid, where the IO/MCM-41 magnetic nanocomposites were dispersed in a nonmagnetic medium oil in addition to as an additive for carbonyl iron-based MR fluid. Their MR properties of flow curve along with yield stress and viscoelastic properties under applied magnetic fields were investigated using a rotational rheometer.

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Acknowledgment

This work was supported by National Research Foundation (#43450-1), Korea (2011).

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Authors and Affiliations

  1. Department of Polymer Science and Engineering, Inha University, Incheon, 402-751, South Korea

    Ying Dan Liu, Bong Jun Park, Fei Fei Fang & Hyoung Jin Choi

  2. Department of Chemical Engineering, Inha University, Incheon, 402-751, South Korea

    Wha-Seung Ahn

  3. State Key Laboratory of Metastable Materials Science and Technology, Yanshan University, Qinhuangdao, 066004, China

    Ying Dan Liu

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  1. Ying Dan Liu
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  2. Bong Jun Park
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  3. Fei Fei Fang
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Correspondence to Hyoung Jin Choi.

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Liu, Y.D., Park, B.J., Fang, F.F. et al. Iron oxide/MCM-41 mesoporous nanocomposites and their magnetorheology. Colloid Polym Sci 291, 1895–1901 (2013). https://doi.org/10.1007/s00396-013-2921-1

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  • DOI: https://doi.org/10.1007/s00396-013-2921-1

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