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Determination of methylbenzo[a]pyrene isomers in a coal tar standard reference material using liquid chromatography and Shpol'skii spectrometry

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Summary

Concentrations of individual methylbenzo[a]pyrene (MBP) isomers were determined in a coal tar standard reference material (SRM 1597) by using liquid chromatography (LC) (normal- and reversed-phase) and high resolution Shpol'skii spectrometry (HRS) at 15 K. This is the first report on the unambiguous identification and quantification of each MBP isomer in a real sample, and this report contains information on the distribution of these highly carcinogenic compounds in coal tar.

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Authors and Affiliations

  1. Groupe d'Océanographie Physico-chimique, UA 348 CNRS Université de Bordeaux I, F-33405, Talence Cedex, France

    Philippe Garrigues & Jacqueline Bellocq

  2. Organic Analytical Research Division, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA

    Stephen A. Wise

Authors
  1. Philippe Garrigues
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  2. Jacqueline Bellocq
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  3. Stephen A. Wise
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Garrigues, P., Bellocq, J. & Wise, S.A. Determination of methylbenzo[a]pyrene isomers in a coal tar standard reference material using liquid chromatography and Shpol'skii spectrometry. Fresenius J Anal Chem 336, 106–110 (1990). https://doi.org/10.1007/BF00322546

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  • DOI: https://doi.org/10.1007/BF00322546

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