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Applications of temperature-resolved diffraction methods in thermal analysis

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Abstract

Fundamentals and fields of application of time- and temperature-resolved diffraction methods are presented. X-ray diffraction and neutron diffraction will be considered. Dynamic diffraction methods are increasingly applied in different fields like solid state reactions, heterogeneous catalysis and biological sciences. New methods like synchrotron radiation and position-sensitive detectors permit a considerable expansion of potential research areas. The dynamic diffraction methods are compared with the classical thermoanalytical methods thermogravimetry and DSC.

Zusammenfassung

Grundlagen und Anwendungsmöglichkeiten zeit-und/oder temperature aufgelöster Beugungsmethoden werden vorgestellt. Dabei wird auf Röntgen- und Neutronenbeugung eingegangen. Dynamische Beugungsmethoden werden zunehmend in verschiedenen Bereichen wie der Festkörperreaktionskinetik, der heterogenen Katalyse und den Biowissenschaften eingesetzt. Der Einsatz neuer Methoden wie der Synchrotronstrahlung und der Ortsempfindlichen Detektoren erlaubt eine erhebliche Erweiterung der Anwendungsgebiete. An ausgewählten Beispielen werden Einsatzmöglichkeiten demonstriert. Die dynamischen Beugungsmethoden werden mit den klassischen thermoanalytischen Techniken Thermogravimetrie und DSC verglichen.

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Epple, M. Applications of temperature-resolved diffraction methods in thermal analysis. Journal of Thermal Analysis 42, 559–593 (1994). https://doi.org/10.1007/BF02548536

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