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Practical liquid chromatographic separation of the phenols in technical cashew nutshell liquid fromAnacardium occidentale

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Lipids

Abstract

The practical separation of cardanol from technical cashew nutshell liquid or its distillate has been effected by liquid chromatography on Silica Gel H 60 (TLC type) with solute/absorbent in the range 1∶5–1∶6. Concentrates of the monoene, diene and triene constituents of cardanol have been prepared by argentation liquid chromatography on Silica Gel H 60 with dry incorporation of 15% silver nitrate. The present use of pressurized columns was made prior to the advent of flash chromatography.

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References

  1. Chan, P., Tyman, J.H.P., and Tychopoulos V., (1984)J. Chromatogr. 303, 137–150.

    Article  Google Scholar 

  2. Tyman, J.H.P., (1979)Chem. Soc. Rev. 8, 499–537.

    Article  CAS  Google Scholar 

  3. Tyman, J.H.P., (1980)Chem. Ind. (London), 59–62.

  4. Ohler, J.G., (1979)Cashew, 1st edn., p. 21, Royal Tropical Institute, Amsterdam.

    Google Scholar 

  5. Durrani, A., Davies, G.L., Sood, S.K., Tychopoulos, V., and Tyman, J.H.P., (1982)J. Chem. Tech. Biotech. 32, 681–690.

    CAS  Google Scholar 

  6. Manzara, A., Patel, M., and Tyman, J.H.P. (1981) US Patent 4352944; UK Patent GB 2066820B.

  7. Tyman, J.H.P., UK Patent Application 8328403, 1985.

  8. Murthy, B.J.G., Sivasamban, S., and Aggarwal, J., (1968)J. Chromatogr. 32, 519–528.

    Article  PubMed  CAS  Google Scholar 

  9. Tyman, J.H.P., (1973)J. Chem. Soc. Perkins Trans. 1, 1639–1647.

    Google Scholar 

  10. Still, W., Kahn, M., and Mitra, A., (1978)J. Org. Chem. 43, 2923–2925.

    Article  CAS  Google Scholar 

  11. Wehrli, A., Hermann, V., and Huber, J.F.K., (1976)J. Chromatogr. 125, 59–70.

    Article  CAS  Google Scholar 

  12. Barford, R.A., McGraw, R., and Rothbarth, H.L., (1978)J. Chromatogr. 166, 365–372.

    Article  CAS  Google Scholar 

  13. Scott, R.P.W., and Kucera, P., (1976)J. Chromatogr. 119, 467–482.

    Article  CAS  Google Scholar 

  14. Tyman, J.H.P., and Morris, L.J., (1967)J. Chromatogr. 27, 287–288.

    Article  CAS  Google Scholar 

  15. Paul, V.J., and Yeddanapalli, L.M., (1956)J. Am. Chem. Soc. 78, 5675–5678.

    Article  CAS  Google Scholar 

  16. Tyman, J.H.P., UK Patent Application 8220097, 1985.

  17. Tyman, J.H.P., and Jacobs, N., (1971)J. Chromatogr. 54, 83–90.

    Article  CAS  Google Scholar 

  18. Dev, S., and Gupta, A.S., (1963)J. Chromatogr. 12, 189–195.

    Article  PubMed  Google Scholar 

  19. Schofield, C.R., (1979)J. Am. Oil Chem. Soc. 56, 510–515.

    Google Scholar 

  20. Tyman, J.H.P., (1975)J. Chromatogr. 111, 277–284.

    Article  CAS  Google Scholar 

  21. Tyman, J.H.P., Tychopoulos, V., and Colenutt, B.A., (1981)J. Chromatogr. 213, 287–300.

    Article  CAS  Google Scholar 

  22. Mitra, A.K., and Pandey, G.N., (1976)Chem. Age India 27, 944–948.

    Google Scholar 

  23. Murthy, B.G.K., Menon, M.C., Aggarwal, J.S., and Zaheer, S.H. (1964)Paint Manuf. 31, 47–52.

    Google Scholar 

  24. Tyman, J.H.P., (1975)J. Chromatogr. 111, 285–292.

    Article  CAS  Google Scholar 

  25. Klawitec, J., Kaminski, M., and Kowalczyk, J.S., (1982)J. Chromatogr. 243, 207–224.

    Article  Google Scholar 

  26. Dawson, C.R., and Symes, W.F., (1953)J. Am. Chem. Soc. 75, 4952–4957.

    Article  Google Scholar 

  27. Baylis, C.J., Odle, S.W.D., and Tyman, J.H.P., (1981)J. Chem. Soc. Perkins Trans. 1, 132–141.

    Google Scholar 

  28. Kashani, M.A. (1978) M. Phil. thesis, Brunel University, Uxbridge, Middlesex, England.

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Authors and Affiliations

  1. Department of Chemistry, Brunel University, UB8 3PH, Uxbridge, Middlesex, England

    Suresh K. Sood, John H. P. Tyman, Aziz Durrani & Robert A. Johnson

Authors
  1. Suresh K. Sood
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  2. John H. P. Tyman
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  3. Aziz Durrani
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  4. Robert A. Johnson
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Additional information

This publication is Part 26 in the series of “Long Chain Phenols”. Reference 1 is Part 25.

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Sood, S.K., Tyman, J.H.P., Durrani, A. et al. Practical liquid chromatographic separation of the phenols in technical cashew nutshell liquid fromAnacardium occidentale . Lipids 21, 241–246 (1986). https://doi.org/10.1007/BF02534830

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  • DOI: https://doi.org/10.1007/BF02534830

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