Summary
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1.
β-Ureido-β-(β-naphthyl)-propionic acid,β-(ω-phenylureido)-β-(β-naphthyl)-propionic acid, andβ-(N1-methylureido)-β-(β-nepthyl)propionic acid have been prepared, and have been converted into the corresponding 2,4-dioxo-hexahydropyrimidine derivatives 6-(β-naphthyl)-dihydrouracil, 3-phenyl-6-(β-naphthyl)-dihydrouracil, and 6-(β-nappthyl)-1-methyl-dihydrouracil.
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2.
Its amide was formed as a by-product of preparation ofβ-ureido-β-(β-napthyl)-propionic acid, and was also synthesized fromβ-amino-β-(β-napthyl)-propionic acid and sodium cyanate.
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3.
β-Ureido-β-(β-naphtyhl)-propionamide undergoes cyclization when heated.
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4.
Methyl-β-(ω-phenylureido)-β-(β-napthyl)-propionate has been prepared.
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5.
2-Thio-6-(β-napthyl)-dihydrouracil,β-guanidino-β-(β-napthyl)-propionic acid, and 4-oxo-β-(β-naphthyl)-2-methyl-3,4,5,6-tetrahydropyrimidine have been synthesized.
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Literature cited
V. M. Rodionov and B. I. Kurtev, Bull. USSR Acad. Sci., Div. Chem. Sci., 1, 113 (1952).
V. M. Rodionov and O. S. Urbanskaya, J. Gen. Chem., 13, 2023 (1948).
V. M. Rodionov and V. K. Zvorykina, Bull. USSR Acad. Sci., Div. Chem. Sci., 216 (1943); 330 (1948); V. M. Rodionoc and V. V. Kiseleva, J. Gen. Chem., 18, 1912 (1948).
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Rodionov, V.M., Kurtev, B.L. 2-(2′-naphthyl)-2-aminoproptonic acid and its pyrimidine derivatives Part 2. Russ Chem Bull 1, 285–291 (1952). https://doi.org/10.1007/BF01170505
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DOI: https://doi.org/10.1007/BF01170505