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Effect of heat treatment conditions on the catalytic graphitization of coal-tar pitch

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Abstract

The effect of heat treatment conditions on the properties of carbon materials obtained in the process of the low-temperature graphitization of coal-tar pitch in the presence of a cellular graphite catalyst was studied by X-ray diffraction and elemental analysis. It was found that materials whose X-ray structural characteristics are close to those of graphite were formed at 800–900°C. An increase in the process temperature to 1400°C, just as an isothermal exposure at 900°C, increased the degree of graphitization of carbon materials but decreased the amount of heteroatoms in their composition.

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References

  1. Iijima, T., Suzuki, K., and Matsuda, Y., Synth. Met., 1995, vol. 73, p. 9.

    Article  CAS  Google Scholar 

  2. Wu, Y.P., Rahm, E., and Holze, R., J.. Power Sources, 2003, vol. 114, p. 228.

    Article  CAS  Google Scholar 

  3. Yamaura, J., Ozaki, Y., Morita, A., and Ohta, A., Abstracts of Papers, 6th Int. Meet. Lithium Batteries, Munster, 1992, p. 103.

    Google Scholar 

  4. Fialkov, A.S., Dubasova, V.S., Nikolenko, A.F., et al., in Fundamental’nye problemy elektrokhimicheskoi energetiki (Fundamental Problems of Electrochemical Power Engineering), Saratov: Izd. Saratov. Gos. Univ., 1999, p. 134.

    Google Scholar 

  5. Yasuda, E., Park, S.-M., Tanabe, Y., et al., Tokyo Inst. Technol., Rept. Res. Lab. Eng. Mater., 1992, no. 17, p. 145.

    Google Scholar 

  6. Taegwhan, H. and Sangjin, H., US Patent 2005/0008562, 2005.

  7. Kodama, Y., Sato, K., and Suzuki, K., et al, Carbon, 2012, vol. 50, no. 10, p. 3486.

    Article  CAS  Google Scholar 

  8. Yasuda, H., Miyanaga, S., Nakamura, A., and Sakai, H., J. Inorg. Organomet. Polym., 1991, vol. 1, no. 1, p. 135.

    Article  CAS  Google Scholar 

  9. Zhang, C., Fransson, M., Liu, C., and Zhou, B., US Patent 2007/0265162, 2007.

  10. Barnakov, Ch.N., Seit-Ablaeva, S.K., Ismagilov, Z.R., et al., RF Patent No. 2429194, Byull. Izobret., 2011, no. 26.

    Google Scholar 

  11. Barnakov, Ch.N., Seit-Ablaeva, S.K., and Ismagilov, Z.R., RF Patent No. 2476374, Byull. Izobret., 2013, no. 6.

    Google Scholar 

  12. Khokhlova, G.P., Malysheva, V.Yu., Barnakov, Ch.N., et al., Vestn. Kuzbass. Gos. Tekhn. Univ., 2013, no. 5, p. 21.

    Google Scholar 

  13. Avdeev V.V., Finaenov A.I., Yakovlev A.V., et al., RF Patent No. 2233794, Byull. Izobret., 2004, no. 22.

    Google Scholar 

  14. Sorokina, N.E., Khaskov, M.A., Avdeev, V.V., and Nikol’skaya, I.V., Zh. Obshch. Khim., 2005, vol. 75, no. 2, p. 184.

    Google Scholar 

  15. Trucano, P. and Chen, R., Nature, 1975, vol. 258, p. 136.

    Article  CAS  Google Scholar 

  16. West, A. R., Solid State Chemistry and Its Applications, New York: John Willey & Sons, 1984, part. 1, ch. 5.

    Google Scholar 

  17. Sherryuble, V.G. and Seleznev, A.N., Pekovyi koks v uglerodnoi promyshlennosti (Pitch Coke in the Carbon Industry), Chelyabinsk: Chelyabinskii Dom Pechati, 2003.

    Google Scholar 

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Correspondence to G. P. Khokhlova.

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Original Russian Text © G.P. Khokhlova, Ch.N. Barnakov, V.Yu. Malysheva, A.N. Popova, Z.R. Ismagilov, 2015, published in Khimiya Tverdogo Topliva, 2015, No. 2, pp. 10–16.

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Khokhlova, G.P., Barnakov, C.N., Malysheva, V.Y. et al. Effect of heat treatment conditions on the catalytic graphitization of coal-tar pitch. Solid Fuel Chem. 49, 66–72 (2015). https://doi.org/10.3103/S0361521915020056

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  • DOI: https://doi.org/10.3103/S0361521915020056

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