Abstract—
New water-soluble SeS2 containing nanocomposites are obtained via ion-exchange interaction between selenous acid and ammonium sulfide in water using natural arabinogalactan and starch polysaccharides as nanoparticle stabilizers. The transmission electron microscopy, X-ray diffraction analysis, and dynamic light scattering data show that nanocomposites are formed as spherical crystalline SeS2 nanoparticles 5–140 nm in size, dispersed in polysaccharide matrices. The type of stabilization matrix and ratio of reactants have a decisive influence on the nanomorphological properties of the materials obtained.
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ACKNOWLEDGMENTS
The equipment of the Collective Usage Center of the Limnological Institute (Siberian Branch, Russian Academy of Sciences) and of the Baikal Analytical Center for Collective Use of the Favorsky Irkutsk Institute of Chemistry (Siberian Branch, Russian Academy of Sciences) was used in this work.
Funding
The study was supported by the Russian Foundation for Basic Research (project no 18-316-20017 mol_a_ved: “Synthesis of SeS2-Containing Nanocomposites and Study of Their Structure”) and the state task of the Favorsky Irkutsk Institute of Chemistry SB RAS (project АААА-А16-116112510011-8: “Study of the Dynamics of Synthesis of Nanocomposites”).
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Translated by A. Tulyabaev
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Lesnichaya, M.V., Sukhov, B.G. Synthesis of Selenium Sulfide Nanoparticles in Polysaccharide Arabinogalactan and Starch Matrices. Nanotechnol Russia 16, 202–210 (2021). https://doi.org/10.1134/S2635167621020099
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DOI: https://doi.org/10.1134/S2635167621020099