Skip to main content
SpringerLink
Log in

Synthesis, crystal structure, and spectral characteristics of N-(tert-butyl)aminomethanesulfonic acid

  • Published:
Russian Journal of General Chemistry Aims and scope Submit manuscript

Abstract

A new method of the synthesis of N-(tert-butyl)aminomethanesulfonic acid in the system SO2–(CH3)3CNH2–CH2O–H2O was developed. The target compound [(CH3)3С]NHCH2SO3H was characterized by means of X-ray diffraction analysis, IR spectroscopy, and mass spectrometry.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. Good, N.E., Winget, G.D., Winter, W., Connolly, T.N., Izawa, S., and Singh, R.M.M., Biochem., 1966, vol. 5, no. 2, p. 467. DOI: 10.1021/bi00866a011.

    Article  CAS  Google Scholar 

  2. Good, N.E., and Izawa, S., Methods Enzymol., 1972, vol. 24, p. 53. DOI: 10.1016/0076-6879(72)24054-x.

    Article  CAS  Google Scholar 

  3. Yu, Q., Kandegedara, A., Xu, Y., and Rorabacher, D.B., Analyt. Biochem., 1997, vol. 253, no. 1, p. 50. DOI: 10.1006/abio.1997. 2349.

    Article  CAS  Google Scholar 

  4. Long, R.D., Hilliard, N.P., Chhatre, S.A., Timofeeva, T.V., Yakovenko, A.A., Dei, D.K., and Mensah, E.A., Beilstein J. Org. Chem., 2010, vol. 6, no. 31. DOI: 10.3762/bjoc.6.31.

    Google Scholar 

  5. Badeev, Yu.V., Korobkova, V.D., Ivanov, V.B., Pozdeev, O.K., Gil’manova, G.Kh., Batyeva, E.S., and Andreev, S.V., Pharm. Chem. J., 1991, vol. 25, no. 4, p. 272. DOI: 10.1007/BF00772113.

    Article  Google Scholar 

  6. Khoma, R.E., Gel’mbol’dt, V.O., Shishkin, O.V., Baumer, V.N., and Koroeva, L.V., Russ. J. Gen. Chem., 2013, vol. 83, no. 5, p. 834. DOI: 10.1134/S1070363213050149.

    Article  Google Scholar 

  7. Khoma, R.E., Shestaka, A.A., Shishkin, O.V., Baumer, V.N., Brusilovskii, Yu.E., Koroeva, L.V., Ennan, A.A., and Gel’mbol’dt, V.O., Russ. J. Gen. Chem., 2011, vol. 81, no. 3, p. 620. DOI: 10.1134/S1070363211030352.

    Article  CAS  Google Scholar 

  8. Sheldrick, G.M., Acta Crystallogr. (A), 2008, vol. 64, no. 1, p. 112. DOI: 10.1107/S0108767307043930.

    Article  CAS  Google Scholar 

  9. Gordon, A.J. and Ford, R.A., The Chemist’s Companion, New York: Wiley, 1972.

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Physicochemical Institute for Human and Environmental Protection, Ministry of Education and Science of the National Academy of Sciences of Ukraine, ul. Preobrazhenskaya 3, Odessa, 65082, Ukraine

    R. E. Khoma & A. A. Ennan

  2. Mechnikov Odessa National University, Odessa, Ukraine

    R. E. Khoma

  3. Odessa National Medical University, Odessa, Ukraine

    V. O. Gel’mbol’dt

  4. Institute of Single Crystals of the National Academy of Sciences of Ukraine, Kharkov, Ukraine

    V. N. Baumer & A. N. Puzan

  5. Karazin Kharkiv National University, Kharkov, Ukraine

    V. N. Baumer

Authors
  1. R. E. Khoma
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. V. O. Gel’mbol’dt
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. A. A. Ennan
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. V. N. Baumer
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. A. N. Puzan
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to R. E. Khoma.

Additional information

Original Russian Text © R.E. Khoma, V.O. Gel’mbol’dt, A.A. Ennan, V.N. Baumer, A.N. Puzan, 2015, published in Zhurnal Obshchei Khimii, 2015, Vol. 85, No. 10, pp. 1650–1652.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Khoma, R.E., Gel’mbol’dt, V.O., Ennan, A.A. et al. Synthesis, crystal structure, and spectral characteristics of N-(tert-butyl)aminomethanesulfonic acid. Russ J Gen Chem 85, 2282–2284 (2015). https://doi.org/10.1134/S1070363215100102

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S1070363215100102

Keywords

Search

Navigation