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Optimization of Cryogenic Treatment Parameters for the Minimum Residual Stress

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Abstract

Residual stress developed after the quenching of aluminum alloys causes distortion during subsequent machining. The purpose of this study was to reduce the residual stress and improve mechanical properties by using a novel cryogenic treatment in an aluminum alloy, specifically, grade 2A12. The orthogonal test and relevant range analysis method were used to optimize cryogenic treatment parameters for improved distribution of residual stress in 2A12 alloy samples. The changes of microstructure were examined by scanning electron microscopy and transmission electron microscope. It was found that the residual stress in 2A12 alloy could be reduced up to 93%, by optimizing the cryogenic treatment parameters, and the reduction was mainly from grain refinement and uniformly distributed S' precipitates ascribing to the cryogenic treatment. The S' precipitates (Al2CuMg) were linked to the formation of Cu-Mg co-clusters, which were broadly equiaxed with no internal order.

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References

  1. Y.B. Dong, W.Z. Shao and X.L. Liang, Numerical Simulation of Residual Stresses in an Al-Cu Alloy Block During Quenching and Aging[J], J. Mater. Eng. Perform., 2015, 24(12), p 4928–4940.

    Article  CAS  Google Scholar 

  2. Z. Zhang, Engineering Materials [M], Tsinghua University Press, Beijing, 2001.

    Google Scholar 

  3. "Non-ferrous metals and their heat treatment" writing group. Colored technology and its heat treatment [M]. Beijing: National Defense Industry Press, 1981.

  4. P.W. Song, Z.Q. He and X.T. Jing, 2A12 aluminum alloy sheet regression heat treatment, Metal Heat Treatment, 2004, 29(10), p 29–31.

    CAS  Google Scholar 

  5. Y.B. Dong, W.Z. Shao and J.T. Jiang, Minimization of Residual Stresses in an Al-Cu Alloy Forged Plate by Different Heat Treatments [J], J. Mater. Eng. Perform., 2015, 24(6), p 2256–2265.

    Article  CAS  Google Scholar 

  6. J.S. Robinson, D.A. Tanner and C.E. Truman, The Influence of Quench Sensitivity on Residual Stresseses in the Aluminium Alloys 7010 and 7075, Mater. Charact., 2012, 65, p 73–85.

    Article  CAS  Google Scholar 

  7. F. Foadian, A. Carrado, T. Pirling et al., Residual Stresses Evolution in Cu Tubes, Cold Drawn with Tilted Dies – Neutron Diffraction Measurements and Finite Element Simulation[J], Mater. Des., 2016, 107, p 163–170.

    Article  CAS  Google Scholar 

  8. L.H. Meng, Study of Residual Stress on the Machined Surface of Ti6Al4V Titanium Alloy [J], J. Mech. Eng., 2019, 055(007), p 64.

    Google Scholar 

  9. Y.W. Lv, X.G. Yan, X.J. Han et al., Effect of Cryogenic Treatment on Residual Stresses of W6Mo5Cr4V2 High Speed Steel, Metal Heat Treatment, 2015, 12, p 89–92.

    Google Scholar 

  10. S. Wu, H. Zhao and A. Lu, A Micro-mechanism Model of Residual Stress Reduction by Low Frequency Alternating Magnetic Field Treatment, J. Mater. Process. Technol., 2003, 132(1), p 198–202.

    Article  CAS  Google Scholar 

  11. F. Lu, X. Tang, J. Luo et al., Research on Residual-Stresses Reduction by Strong Pulsed Magnetic Treatment, J. Mater. Process. Technol., 1998, 74(1), p 259–262.

    Article  Google Scholar 

  12. J.S. Robinson, D.A. Tanner, S. Van Petegem et al., Influence of Quenching and Aging on Residual Stress in Al-Zn-Mg-Cu Alloy 7449[J], Mater. Sci. Technol., 2012, 28(4), p 420–430.

    Article  CAS  Google Scholar 

  13. Xu LY, Zhu J, Jing HY. Effects of deep cryogenic treatment on the residual stress and mechanical properties of electron-beam-welded Ti-6Al-4V joints [J]. Materials Science & Engineering A Structural Materials Properties Misrostructure & Processing, 2016.

  14. M. Koneshlou, K.M. Asl and F. Khomamizadeh, Effect of Cryogenic Treatment on Microstructure, Mechanical and Wear Behaviors of AISI H13 Hot Work Tool Steel, Cryogenics, 2011, 51(1), p 55–61.

    Article  CAS  Google Scholar 

  15. A. Molinari, M. Pellizzari, S. Gialanella et al., Effect of Deep Cryogenic Treatment on the Mechanical Properties of Tool Steels, J. Mater. Process. Technol., 2001, 118(1–3), p 350–355.

    Article  CAS  Google Scholar 

  16. A. Bensely, S. Venkatesh, D.M. Lal et al., Effect of Cryogenic Treatment on Distribution of Residual Stress in Case Carburized En 353 Steel, Mater. Sci. Eng., A, 2008, 479(1–2), p 229–235.

    Article  Google Scholar 

  17. H.J. Lim, D.H. Ko, D.C. Ko et al., Reduction of Residual Stress and Improvement of Dimensional Accuracy by Uphill Quenching for Al6061 Tube[J], Metall. Mater. Trans. B., 2014, 45(2), p 472–481.

    Article  CAS  Google Scholar 

  18. Z.G. Nie, G. Wang, Y.L. Lin et al., Precision Measurement and Modeling of Quenching-Tempering Distortion in Low-Alloy Steel Components with Internal Threads[J], J. Mater. Eng. Perform., 2015, 24(12), p 4878–4889.

    Article  CAS  Google Scholar 

  19. Q.C. Wang and Y.L. Ke, Study on Eliminating Residual Stress of 7050 Aluminum Alloy by Cryogenic Treatment [J], J. Zhejiang Univ. (Eng. Ed), 2003, 06, p 120–123.

    Google Scholar 

  20. Li JJ, Yan XG, Liang XY, et al. TEMPORARY REMOVAL: Influence of different cryogenic treatments on high-temperature wear behavior of M2 steel [J]. Wear, 2017:S0043164816308778.

  21. B. Wang, R. Lin, D. Liu, J. Xu et al., Investigation of the Effect of Humidity at Both Electrode on the Performance of PEMFC Using Orthogonal Test Method, Int. J. Hydrog. Energy, 2019, 44, p 13737–13743.

    Article  CAS  Google Scholar 

  22. R. Lin, X. Diao, T. Ma et al., Optimized Microporous Layer for Improving Polymer Exchange Membrane Fuel Cell Performance Using Orthogonal Test Design, Appl. Energy, 2019, 254, p 113714.

    Article  CAS  Google Scholar 

  23. Protoxrd Inc., Proto-iXRD combo system user manual, Italy, 2010.

  24. J. Robinson, D.A. Tanner, S.V. Petegem et al., Influence of Quenching and Aging on Residual Stresses in Al–Zn–Mg–Cu Alloy 7449, Mater. Sci. Technol., 2012, 28(4), p 420–430.

    Article  CAS  Google Scholar 

  25. W.D. Zhang, P.K. Bai, J. Yang et al., Tensile Behavior of 3104 Aluminum Alloy Processed by Homogenization and Cryogenic Treatment, Trans. Nonferrous Metals Soc. China, 2014, 24(8), p 2453–2458.

    Article  CAS  Google Scholar 

  26. J. Robinson, D.A. Tanner, C.E. Truman et al., The Influence of Quench Sensitivity on Residual Stresses in the Aluminium Alloys 7010 and 7075, Mater. Charact., 2012, 65, p 73–85.

    Article  CAS  Google Scholar 

  27. Y.S. Sun, F.L. Jiang, H. Zhang et al., Residual stresses relief in Al–Zn–Mg–Cu alloy by a new multistage interrupted artificial aging treatment [J], Mater. Des., 2016, 92, p 281–287.

    Article  CAS  Google Scholar 

  28. M. Araghchi, H. Mansouri, R. Vafaei and Y. Guo, A Novel Cryogenic Treatment for Reduction of Residual Stresses in 2024 Aluminum Alloy, Mater. Sci. Eng. A, 2017, 689, p 48–52.

    Article  CAS  Google Scholar 

  29. Y.C. Lin, Y.Q. Jiang, Y.C. Xia et al., Effects of Creep-aging Processing on the Corrosion Resistance and Mechanical Properties of an Al–Cu–Mg Alloy[J], Mater. Sci. Eng. A, 2014, 605, p 192–202.

    Article  CAS  Google Scholar 

  30. W.L. Gao, X.J. Wang, J.Z. Chen et al., Effect of Cryogenic Treatment on Peak Aging Precipitates of 7A99 Aluminum Alloy[J], Rare Metal Mater. Eng., 2019, 48(4), p 1155–1160.

    Google Scholar 

  31. W.J. Ma, Z.G. Chen, H.J. Li et al., Process and Mechanism of Novel Heat Treatment for Regulating Residual Stresses in Al-Cu-Mg alloys[J], J. Mater. Res., 2019, 33(06), p 435–442.

  32. Y.J. Wang, W. Sun, P.W. Li et al., Influence of Cryogenic Treatment on Microstructure and Properties of 2024 Aluminum Alloy Extruded Bar, Light Alloy Process. Technol., 2012, 40(09), p 56–59.

    Google Scholar 

  33. G.X. Hu, X. Cai and Y.H. Rong, Fundamentals of Materials Science [M], Shanghai Jiaotong University Press, China, 2010.

    Google Scholar 

  34. Yang Y, Li RX, Zhang WH, et al.Effects of cryogenic treatment on microstructure and properties of Al-Si-Cu-Mg alloy [C], Symposium of 2014 Chinese Foundry Activity Week, Zhengzhou, 2014, p 1–6

  35. Z.Q. Tian, K.X. Wei, W. Wei et al., Microstructure and Mechanical Properties of Cryogenic Aluminum Silicon Alloy [J], Metal Heat Treatment, 2017, 42(02), p 54–58.

    CAS  Google Scholar 

  36. C.X. Guo and Z.C. Li, Effect of Cryogenic Treatment on Microstructure and Properties of ZL109 [J], Hot Working Process, 2005, 10, p 40–41.

    Google Scholar 

  37. K. Mohan, J.A. Suresh, P. Ramu et al., Microstructure and Mechanical Behavior of Al 7075–T6 Subjected to Shallow Cryogenic Treatment[J], J. Mater. Eng. Perform., 2016, 25(6), p 2185–2194.

    Article  CAS  Google Scholar 

Download references

Acknowledgment

The authors gratefully acknowledge the support of the PhD Start-up Foundation at the Taiyuan University of Science and Technology, China (20182035); Jincheng Science and Technology Plan Project, China ( 20198025); Excellent Graduate Innovation Project of Shanxi Province, China(2019SY476).

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Correspondence to Yao Huang.

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Niu, X., Huang, Y., Yan, X. et al. Optimization of Cryogenic Treatment Parameters for the Minimum Residual Stress. J. of Materi Eng and Perform 30, 9038–9047 (2021). https://doi.org/10.1007/s11665-021-06136-x

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  • DOI: https://doi.org/10.1007/s11665-021-06136-x

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