Abstract
Residual stress developed after the quenching of aluminum alloys causes distortion during subsequent machining. The purpose of this study was to reduce the residual stress and improve mechanical properties by using a novel cryogenic treatment in an aluminum alloy, specifically, grade 2A12. The orthogonal test and relevant range analysis method were used to optimize cryogenic treatment parameters for improved distribution of residual stress in 2A12 alloy samples. The changes of microstructure were examined by scanning electron microscopy and transmission electron microscope. It was found that the residual stress in 2A12 alloy could be reduced up to 93%, by optimizing the cryogenic treatment parameters, and the reduction was mainly from grain refinement and uniformly distributed S' precipitates ascribing to the cryogenic treatment. The S' precipitates (Al2CuMg) were linked to the formation of Cu-Mg co-clusters, which were broadly equiaxed with no internal order.
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References
Y.B. Dong, W.Z. Shao and X.L. Liang, Numerical Simulation of Residual Stresses in an Al-Cu Alloy Block During Quenching and Aging[J], J. Mater. Eng. Perform., 2015, 24(12), p 4928–4940.
Z. Zhang, Engineering Materials [M], Tsinghua University Press, Beijing, 2001.
"Non-ferrous metals and their heat treatment" writing group. Colored technology and its heat treatment [M]. Beijing: National Defense Industry Press, 1981.
P.W. Song, Z.Q. He and X.T. Jing, 2A12 aluminum alloy sheet regression heat treatment, Metal Heat Treatment, 2004, 29(10), p 29–31.
Y.B. Dong, W.Z. Shao and J.T. Jiang, Minimization of Residual Stresses in an Al-Cu Alloy Forged Plate by Different Heat Treatments [J], J. Mater. Eng. Perform., 2015, 24(6), p 2256–2265.
J.S. Robinson, D.A. Tanner and C.E. Truman, The Influence of Quench Sensitivity on Residual Stresseses in the Aluminium Alloys 7010 and 7075, Mater. Charact., 2012, 65, p 73–85.
F. Foadian, A. Carrado, T. Pirling et al., Residual Stresses Evolution in Cu Tubes, Cold Drawn with Tilted Dies – Neutron Diffraction Measurements and Finite Element Simulation[J], Mater. Des., 2016, 107, p 163–170.
L.H. Meng, Study of Residual Stress on the Machined Surface of Ti6Al4V Titanium Alloy [J], J. Mech. Eng., 2019, 055(007), p 64.
Y.W. Lv, X.G. Yan, X.J. Han et al., Effect of Cryogenic Treatment on Residual Stresses of W6Mo5Cr4V2 High Speed Steel, Metal Heat Treatment, 2015, 12, p 89–92.
S. Wu, H. Zhao and A. Lu, A Micro-mechanism Model of Residual Stress Reduction by Low Frequency Alternating Magnetic Field Treatment, J. Mater. Process. Technol., 2003, 132(1), p 198–202.
F. Lu, X. Tang, J. Luo et al., Research on Residual-Stresses Reduction by Strong Pulsed Magnetic Treatment, J. Mater. Process. Technol., 1998, 74(1), p 259–262.
J.S. Robinson, D.A. Tanner, S. Van Petegem et al., Influence of Quenching and Aging on Residual Stress in Al-Zn-Mg-Cu Alloy 7449[J], Mater. Sci. Technol., 2012, 28(4), p 420–430.
Xu LY, Zhu J, Jing HY. Effects of deep cryogenic treatment on the residual stress and mechanical properties of electron-beam-welded Ti-6Al-4V joints [J]. Materials Science & Engineering A Structural Materials Properties Misrostructure & Processing, 2016.
M. Koneshlou, K.M. Asl and F. Khomamizadeh, Effect of Cryogenic Treatment on Microstructure, Mechanical and Wear Behaviors of AISI H13 Hot Work Tool Steel, Cryogenics, 2011, 51(1), p 55–61.
A. Molinari, M. Pellizzari, S. Gialanella et al., Effect of Deep Cryogenic Treatment on the Mechanical Properties of Tool Steels, J. Mater. Process. Technol., 2001, 118(1–3), p 350–355.
A. Bensely, S. Venkatesh, D.M. Lal et al., Effect of Cryogenic Treatment on Distribution of Residual Stress in Case Carburized En 353 Steel, Mater. Sci. Eng., A, 2008, 479(1–2), p 229–235.
H.J. Lim, D.H. Ko, D.C. Ko et al., Reduction of Residual Stress and Improvement of Dimensional Accuracy by Uphill Quenching for Al6061 Tube[J], Metall. Mater. Trans. B., 2014, 45(2), p 472–481.
Z.G. Nie, G. Wang, Y.L. Lin et al., Precision Measurement and Modeling of Quenching-Tempering Distortion in Low-Alloy Steel Components with Internal Threads[J], J. Mater. Eng. Perform., 2015, 24(12), p 4878–4889.
Q.C. Wang and Y.L. Ke, Study on Eliminating Residual Stress of 7050 Aluminum Alloy by Cryogenic Treatment [J], J. Zhejiang Univ. (Eng. Ed), 2003, 06, p 120–123.
Li JJ, Yan XG, Liang XY, et al. TEMPORARY REMOVAL: Influence of different cryogenic treatments on high-temperature wear behavior of M2 steel [J]. Wear, 2017:S0043164816308778.
B. Wang, R. Lin, D. Liu, J. Xu et al., Investigation of the Effect of Humidity at Both Electrode on the Performance of PEMFC Using Orthogonal Test Method, Int. J. Hydrog. Energy, 2019, 44, p 13737–13743.
R. Lin, X. Diao, T. Ma et al., Optimized Microporous Layer for Improving Polymer Exchange Membrane Fuel Cell Performance Using Orthogonal Test Design, Appl. Energy, 2019, 254, p 113714.
Protoxrd Inc., Proto-iXRD combo system user manual, Italy, 2010.
J. Robinson, D.A. Tanner, S.V. Petegem et al., Influence of Quenching and Aging on Residual Stresses in Al–Zn–Mg–Cu Alloy 7449, Mater. Sci. Technol., 2012, 28(4), p 420–430.
W.D. Zhang, P.K. Bai, J. Yang et al., Tensile Behavior of 3104 Aluminum Alloy Processed by Homogenization and Cryogenic Treatment, Trans. Nonferrous Metals Soc. China, 2014, 24(8), p 2453–2458.
J. Robinson, D.A. Tanner, C.E. Truman et al., The Influence of Quench Sensitivity on Residual Stresses in the Aluminium Alloys 7010 and 7075, Mater. Charact., 2012, 65, p 73–85.
Y.S. Sun, F.L. Jiang, H. Zhang et al., Residual stresses relief in Al–Zn–Mg–Cu alloy by a new multistage interrupted artificial aging treatment [J], Mater. Des., 2016, 92, p 281–287.
M. Araghchi, H. Mansouri, R. Vafaei and Y. Guo, A Novel Cryogenic Treatment for Reduction of Residual Stresses in 2024 Aluminum Alloy, Mater. Sci. Eng. A, 2017, 689, p 48–52.
Y.C. Lin, Y.Q. Jiang, Y.C. Xia et al., Effects of Creep-aging Processing on the Corrosion Resistance and Mechanical Properties of an Al–Cu–Mg Alloy[J], Mater. Sci. Eng. A, 2014, 605, p 192–202.
W.L. Gao, X.J. Wang, J.Z. Chen et al., Effect of Cryogenic Treatment on Peak Aging Precipitates of 7A99 Aluminum Alloy[J], Rare Metal Mater. Eng., 2019, 48(4), p 1155–1160.
W.J. Ma, Z.G. Chen, H.J. Li et al., Process and Mechanism of Novel Heat Treatment for Regulating Residual Stresses in Al-Cu-Mg alloys[J], J. Mater. Res., 2019, 33(06), p 435–442.
Y.J. Wang, W. Sun, P.W. Li et al., Influence of Cryogenic Treatment on Microstructure and Properties of 2024 Aluminum Alloy Extruded Bar, Light Alloy Process. Technol., 2012, 40(09), p 56–59.
G.X. Hu, X. Cai and Y.H. Rong, Fundamentals of Materials Science [M], Shanghai Jiaotong University Press, China, 2010.
Yang Y, Li RX, Zhang WH, et al.Effects of cryogenic treatment on microstructure and properties of Al-Si-Cu-Mg alloy [C], Symposium of 2014 Chinese Foundry Activity Week, Zhengzhou, 2014, p 1–6
Z.Q. Tian, K.X. Wei, W. Wei et al., Microstructure and Mechanical Properties of Cryogenic Aluminum Silicon Alloy [J], Metal Heat Treatment, 2017, 42(02), p 54–58.
C.X. Guo and Z.C. Li, Effect of Cryogenic Treatment on Microstructure and Properties of ZL109 [J], Hot Working Process, 2005, 10, p 40–41.
K. Mohan, J.A. Suresh, P. Ramu et al., Microstructure and Mechanical Behavior of Al 7075–T6 Subjected to Shallow Cryogenic Treatment[J], J. Mater. Eng. Perform., 2016, 25(6), p 2185–2194.
Acknowledgment
The authors gratefully acknowledge the support of the PhD Start-up Foundation at the Taiyuan University of Science and Technology, China (20182035); Jincheng Science and Technology Plan Project, China ( 20198025); Excellent Graduate Innovation Project of Shanxi Province, China(2019SY476).
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Niu, X., Huang, Y., Yan, X. et al. Optimization of Cryogenic Treatment Parameters for the Minimum Residual Stress. J. of Materi Eng and Perform 30, 9038–9047 (2021). https://doi.org/10.1007/s11665-021-06136-x
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DOI: https://doi.org/10.1007/s11665-021-06136-x