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An Experimental Investigation of Effects of Fluxes (Na3AlF6 and K2TiF6), Element Alloys (Mg), and Composite Powders ((Al + TiC)CP and (Al + B4C)CP) on Distribution of Particles and Phases in Al-B4C and Al-TiC Composites

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Abstract

The wettability, incorporation, and gravity segregation of TiC and B4C particles into molten aluminum are important problems in the production of Al-TiC and Al-B4C composites by the casting techniques. In order to solve these problems, different methods consisting of adding the Na3AlF6 and K2TiF6 fluxes and Mg (as the alloying element) into the molten aluminum and injection of the (Al + TiC)CP and (Al + B4C)CP composite powders instead of B4C and TiC particles are evaluated. In this work, the conditions of sample preparation, such as particle addition temperature, stirring speed, and stirring time, are determined after many studies and tests. Microstructural characterizations of samples are investigated by scanning electron microscopy equipped with energy dispersive spectroscopy (EDS) and X-ray diffractometry. The results show better distribution and incorporation of TiCp and B4Cp in aluminum matrix when the fluxes are used, as well as EDS analysis of the interface between the matrix and reinforcement-strengthened formation of the different phases such as Al4C3 in the Al-TiC composites and Al3BC, TiB2 in the Al-B4C composites.

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References

  1. Q. Zhang, G. Wu, G. Chen, L. Jiang, and B. Luan: Compos. Part A, 2003, vol. 34, pp. 1023–27.

    Article  Google Scholar 

  2. K.M. Shorowordi, T. Laoui, A.S.M.A. Haseeb, J.P. Celis, and L. Froyen: Mater. Proc. Technol., 2003, vol. 142, pp. 738–43.

    Article  Google Scholar 

  3. H.R. Lashgari, M. Emamy, A. Razaghian, and A.A. Najimi: Mater. Sci. Eng. A, 2009, vol. 517, pp. 170–79.

    Article  Google Scholar 

  4. F. Toptan, A. Kilicarslan, A. Karaaslan, M. Cigdem, and I. Kerti: Mater. Des., 2010, vol. 31, pp. 87–91.

    Article  Google Scholar 

  5. J. Ye, J. He, and J.M. Schoenung: Metall. Mater. Trans. A, 2006, vol. 37, pp. 3099–3109.

    Article  Google Scholar 

  6. E. Frase, S. Wierzbinski, A. Janas, and H.F. Lopez: Metall. Mater. Trans. A, 2002, vol. 33A, pp. 3831–38.

    Article  Google Scholar 

  7. S. Sheibani and M. Fazel Najafabadi: Mater. Des., 2007, vol. 28, pp. 2373–78.

    Article  Google Scholar 

  8. C. Selcuk and A.R. Kennedy: Mater. Lett., 2006, vol. 60, pp. 3364–66.

    Article  Google Scholar 

  9. S.N. Chou, J.L. Huang, D.F. Lii, and H.H. Lu: J. Alloys Compd., 2007, vol. 436, pp. 124–30.

    Article  Google Scholar 

  10. A.A. Hamid, S.C. Jain, P.K. Ghosh, and S. Ray: Metall. Mater. Trans. B, 2006, vol. 37, pp. 519–29.

    Article  Google Scholar 

  11. S.B. Venkata Siva, K.L. Sahoo, R.I. Ganguly, R.R. Dash, S.K. Singh, B.K. Satpathy, and G. Srinivasarao: Metall. Mater. Trans. B, 2013, vol. 44, pp. 800–08.

    Article  Google Scholar 

  12. X.X. Zhang, C.F. Deng, Y.B. Shen, D.Z. Wang, and L. Geng: Mater. Lett., 2007, vol. 61, pp. 3504–06.

    Article  Google Scholar 

  13. S. Jerome, B. Ravisankar, P. Kumar Mahato, and S. Natarajan: Tribol. Int., 2010, vol. 43, pp. 2029–36.

    Article  Google Scholar 

  14. I. Kerti and F. Toptan: Mater. Lett., 2008, vol. 62, pp. 1215–18.

    Article  Google Scholar 

  15. A. Contreras, E. Bedolla, and R. Perez: Acta Mater., 2004, vol. 52, pp. 985–94.

    Article  Google Scholar 

  16. P. Li, E.G. Kandalova, and V.I. Nikitin: Mater. Lett., 2005, vol. 59, pp. 2545–48.

    Article  Google Scholar 

  17. V.H. Lopez and A.R. Kennedy: J. Coll. Interface Sci., 2006, vol. 298, pp. 356–62.

    Article  Google Scholar 

  18. E.A. Aguilar, C.A. Leon, A. Contreras, V.H. Lopez, and R.A.L. Drew, and E. Bedolla: Compos. Part A, 2002, vol. 33, pp. 1425–28.

    Article  Google Scholar 

  19. S. Amirkhanlou and B. Niroumand: Trans. Nonferrous. Met. Soc. China, 2010, vol. 20, pp. 788–93.

    Article  Google Scholar 

  20. N. Frumin, N. Frage, M. Polak, and M.P. Dariel: Scripta Mater., 1997, vol. 37, pp. 1263–71.

    Article  Google Scholar 

  21. N. Eustathopoulos: Acta Mater., 1998, vol. 46, pp. 2319–27.

    Google Scholar 

  22. K.B. Lee, H.S. Sim, S.Y. Cho, and H. Kwon: Mater. Sci. Eng. A, 2001, vol. 302, pp. 227–34.

    Article  Google Scholar 

  23. J. Hashim, L. Looney, and M.S.J. Hashmi: J. Mater. Process. Technol., 2001, vol. 119, pp. 324–28.

    Article  Google Scholar 

  24. A.R. Kennedy and S.M. Wyatt: Compos. Part A, 2001, vol. 32, pp. 555–59.

    Article  Google Scholar 

  25. J.G. Li: Ceram. Int., 1994, vol. 20, pp. 391–412.

    Article  Google Scholar 

  26. K.M. Asif Iqbal, Y. Arai, and W. Arak: Compos. Mater., 2013, vol. 3, pp. 97–106.

    Google Scholar 

  27. S.J. Hong, H.M. Kim, D. Huh, C. Suryanarayana, and B.S. Chun: Mater. Sci. Eng. A, 2003, vol. 347, pp. 198–204.

    Article  Google Scholar 

  28. A. Contreras, C. Angeles Chavez, O. Flores, and R. Perez: Mater. Charact., 2007, vol. 58, pp. 685–93

    Article  Google Scholar 

  29. A. Contreras, C.A. Leon, R.A.L. Drew, and E. Bedolla: Scripta Mater., 2003, vol. 48, pp. 1625–30.

    Article  Google Scholar 

  30. Y. Mazaheri, M. Meratian, R. Emadi, and A.R. Najarian: Mater. Sci. Eng. A, 2013, vol. 560, pp. 278–87.

    Article  Google Scholar 

  31. A.R. Kennedy and B. Brampton: Scripta Mater., 2001, vol. 44, pp. 1077–82.

    Article  Google Scholar 

  32. G. Arslan, F. Kara, and S. Turan: Eur. Ceram. Soc., 2003, vol. 23, pp. 1243–55.

    Article  Google Scholar 

  33. N. Frage, L. Levin, N. Frumin, M. Gelbstein, and M.P. Dariel: Mater. Proc. Technol., 2003, vols. 143–144, pp. 486–90.

    Article  Google Scholar 

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Correspondence to Younes Mazaheri.

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Manuscript submitted August 22, 2016.

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Mazaheri, Y., Emadi, R., Meratian, M. et al. An Experimental Investigation of Effects of Fluxes (Na3AlF6 and K2TiF6), Element Alloys (Mg), and Composite Powders ((Al + TiC)CP and (Al + B4C)CP) on Distribution of Particles and Phases in Al-B4C and Al-TiC Composites. Metall Mater Trans B 48, 1279–1291 (2017). https://doi.org/10.1007/s11663-016-0900-x

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