Abstract
This work presents mechanical properties of the NiTi polycrystalline superelastic shape memory alloys (SMA) of 5 different grain sizes under high-speed impacts. The amorphous, nanocrystalline (40, 80, 120 nm) and coarse grain (20 μm) sheets are manufactured with cold rolling and suitable heat treatments. A Hopkinson tensile bar is used to perform tests up to 45 m/s. High-speed camera system and digital image correlation method are used to get the strain field and particle velocity field at a sampling frequency of 2×106 frames/s with a resolution of 924×768 pixels. Nominal stress-strain curves are obtained for all the sheets with a strain rate of about 1000 s−1 and they have a similar evolution to the quasi-static case but with much higher stress levels. The rate sensitivity is increased with the grain size and the stress level can reach up to a 70% growth for a coarse grain sheet but be totally insensitive for the amorphous sheet in the strain rate from 10−4 to 103 s−1. A single transformation front can be found under high-speed impact (45 m/s) at the early loading stage. The speed of the transformation front is calculated from strain time histories and the highest front speed of 811 m/s is observed which is never observed before. It also reveals that the front speed depends also on the grain size. With the same loading speed, the bigger the grain size is, the slower the transformation front speed is.
Similar content being viewed by others
References
Bhattacharya K. Microstructure of Martensite: Why It Forms and How It Gives Rise to the Shape-Memory Effect. Oxford: Oxford University Press, 2003
Lagoudas D C. Shape Memory Alloys: Modeling and Engineering Applications. Cham: Springer, 2008
Shaw J. Thermomechanical aspects of NiTi. J Mech Phys Solids, 1995, 43: 1243–1281
Shaw J A, Kyriakides S. On the nucleation and propagation of phase transformation fronts in a NiTi alloy. Acta Mater, 1997, 45: 683–700
Zhang X, Feng P, He Y, et al. Experimental study on rate dependence of macroscopic domain and stress hysteresis in NiTi shape memory alloy strips. Int J Mech Sci, 2010, 52: 1660–1670
Pieczyska E A, Gadaj S P, Nowacki W K, et al. Phase-transformation fronts evolution for stress- and strain-controlled tension tests in TiNi shape memory alloy. Exp Mech, 2006, 46: 531–542
Nemat-Nasser S, Choi J Y. Strain rate dependence of deformation mechanisms in a Ni-Ti-Cr shape-memory alloy. Acta Mater, 2005, 53: 449–454
Nemat-Nasser S, Choi J Y, Guo W G, et al. Very high strain-rate response of a NiTi shape-memory alloy. Mech Mater, 2005, 37: 287–298
Adharapurapu R R, Jiang F, Vecchio K S, et al. Response of NiTi shape memory alloy at high strain rate: A systematic investigation of temperature effects on tension-compression asymmetry. Acta Mater, 2006, 54: 4609–4620
Huang H, Durand B, Sun Q P, et al. An experimental study of NiTi alloy under shear loading over a large range of strain rates. Int J Impact Eng, 2017, 108: 402–413
Niemczura J, Ravi-Chandar K. Dynamics of propagating phase boundaries in NiTi. J Mech Phys Solids, 2006, 54: 2136–2161
Escobar J C, Clifton R J, Yang S Y. Stress-wave-induced martensitic phase transformations in NiTi. Shock Compress Condens Matter, 1999, 267: 267–270
Xiao R, Hou B, Sun Q P, et al. An experimental investigation of the nucleation and the propagation of NiTi martensitic transformation front under impact loading. Int J Impact Eng, 2020, 140: 103559
Waitz T, Kazykhanov V, Karnthaler H P. Martensitic phase transformations in nanocrystalline NiTi studied by TEM. Acta Mater, 2004, 52: 137–147
Kim Y, Cho G, Hur S, et al. Nanocrystallization of a Ti-50.0Ni(at.%) alloy by cold working and stress/strain behavior. Mater Sci Eng-A, 2006, 438–440: 531–535
Ahadi A, Sun Q. Effects of grain size on the rate-dependent thermomechanical responses of nanostructured superelastic NiTi. Acta Mater, 2014, 76: 186–197
Xia M, Liu P, Sun Q. Grain size dependence of Young’s modulus and hardness for nanocrystalline NiTi shape memory alloy. Mater Lett, 2018, 211: 352–355
Mei Q S, Zhang L, Tsuchiya K, et al. Grain size dependence of the elastic modulus in nanostructured NiTi. Scr Mater, 2010, 63: 977–980
Shi X B, Guo F M, Zhang J S, et al. Grain size effect on stress hysteresis of nanocrystalline NiTi alloys. J Alloys Compd, 2016, 688: 62–68
Polatidis E, Šmid M, Kuběna I, et al. Deformation mechanisms in a superelastic NiTi alloy: An in-situ high resolution digital image correlation study. Mater Des, 2020, 191: 108622
Wang X, Li C, Verlinden B, et al. Effect of grain size on aging microstructure as reflected in the transformation behavior of a low-temperature aged Ti-50.8at.% Ni alloy. Scr Mater, 2013, 69: 545–548
Tilak Kumar J V, Jayaprakasam S, Padmanabhan K A, et al. On the tensile behaviour of coarse and ultrafine grained NiTi. Mater Charact, 2019, 149: 41–51
Ahadi A, Sun Q. Stress hysteresis and temperature dependence of phase transition stress in nanostructured NiTi—Effects of grain size. Appl Phys Lett, 2013, 103: 021902
Zhao H, Gary G. On the use of SHPB techniques to determine the dynamic behavior of materials in the range of small strains. Int J Solids Struct, 1996, 33: 3363–3375
Hopkinson B. A method of measuring the pressure produced in the detonation of high, explosives or by the impact of bullets. Phil Trans R Soc Lond A, 1914, 213: 437–456
Kolsky H. An investigation of the mechanical properties of materials at very high rates of loading. Proc Phys Soc B, 1949, 62: 676–700
Xiao R, Hou B, Sun Q P, et al. A numerical investigation of the nucleation and the propagation of NiTi martensitic transformation front under impact loading. Int J Impact Eng, 2021, 152: 103841
Author information
Authors and Affiliations
Corresponding author
Additional information
This work was supported by the National Natural Science Foundation of China (Grant No. 11972310).
Rights and permissions
About this article
Cite this article
Xiao, R., Hou, B., Sun, Q. et al. Mechanical behaviors of polycrystalline NiTi SMAs of various grain sizes under impact loading. Sci. China Technol. Sci. 64, 1401–1411 (2021). https://doi.org/10.1007/s11431-020-1798-4
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11431-020-1798-4