Abstract
Reaction of bis(aminofurazanyl)furoxan with 2,2-dimethyl-5-nitro-5-nitroso-1,3-dioxane in the presence of dibromoisocyanurate and a series of subsequent transformations give rise to the following bis(mononitroalkyland polynitromethyl-ONN-azoxyfurazanyl)furoxans: bis(nitromethyl-ONN-azoxyfurazanyl)furoxan, bis(dinitromethyl-ONN-azoxyfurazanyl)furoxan, bis(trinitromethyl-ONN-azoxyfurazanyl)furoxan, and a number of their derivatives, including bis(fluorodinitrometyl-ONN-azoxyfurazanyl)furoxan.
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Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 1, pp. 0137–0141, January, 2015.
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Luk’yanov, O.A., Pokhvisneva, G.V. & Ternikova, T.V. Nitro-substituted bis(methyl-ONN-azoxyfurazanyl)furoxans. Russ Chem Bull 64, 137–141 (2015). https://doi.org/10.1007/s11172-015-0832-7
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DOI: https://doi.org/10.1007/s11172-015-0832-7
Keywords
- bis(α-nitroalkyl-ONN-azoxyfurazanyl)furoxans
- bis(halonitromethyl-ONNazoxyfurazanyl)furoxans
- bis(nitromethyl-ONN-azoxyfurazanyl)furoxan
- bis(dinitromethylONN-azoxyfurazanyl)furoxan
- bis(trinitromethyl-ONN-azoxyfurazanyl)furoxan
- bis(fluorodinitromethyl-ONN-azoxyfurazanyl)furoxan
- nitration
- bromination
- debromination
- deoxymethylation