Abstract
Spheroidal growth of silicon carbide (SiC) was observed by treating SiC grain in thermal arc plasma reactor/furnace followed by 4 h of in situ cooling under argon atmosphere. The plasma treatment of samples was carried out between 5 and 15 min. under Ar atmosphere. High microhardness and Young’s modulus values were found for plasma-treated SiC with spheroidal structure. Materials were evaluated by employing techniques such as XRD, XPS, micro Raman, FTIR, FESEM, TEM, EDS, microhardness, and Young’s modulus. Typical 15 min. plasma-treated SiC shows relatively high microhardness and Young’s modulus values of 3680 VHN and 470 GPa, respectively, than that of untreated one.
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References
Barghi SH, Tsotsis TT, Sahimi M (2015) Hydrogen absorption in silicon carbide nanotubes doped with potassium and titanium. AIChE Annual Meeting; 8–3 November, Salt Lake City, UT, USA
Harris GL (1995) Properties of silicon carbide. Iet
Lee JT et al (2013) Sulfur-infiltrated micro-and mesoporous silicon carbide-derived carbon cathode for high-performance lithium sulfur batteries. Adv Mater 25(33):4573–4579
Sahu RK et al (2019) Production of C/SiC nanotubes by arc Plasma treatment. Mat Today: Proc 18:575–581
Nayak BB et al (2018) Growth of silicon carbide nanotubes in arc plasma treated silicon carbide grains and their microstructural characterizations. Ceram Int 4:1512–1517
Son IH et al (2015) Silicon carbide-free graphene growth on silicon for lithium-ion battery with high volumetric energy density. Nature Comm 6:7393
Petrovic J et al (1985) Tensile mechanical properties of SiC whiskers. J Mat Sci 20(4):1167–1177
Brennan JJ, Prewo KM (1982) Silicon carbide fibre reinforced glass-ceramic matrix composites exhibiting high strength and toughness. J Mat Sci 17(8):2371–2383
Pham-Huu C et al (2001) The first preparation of silicon carbide nanotubes by shape memory synthesis and their catalytic potential. J Catal 200(2):400–410
Yang W et al (2004) Synthesis of silicon carbide nanorods by catalyst-assisted pyrolysis of polymeric precursor. Chem Phys Lett 383(5–6):441–444
Keller N, et al (2005) New catalysts based on silicon carbide support for improvements in the sulfur recovery. Silicon carbide as support for the selective H2S oxidation. J Brazilian Chem Soc 16(2):202–209
Mavrandonakis A et al (2006) Silicon carbide nanotube tips: promising materials for atomic force microscopy and/or scanning tunneling microscopy. Appl Phys Lett 89(12): 123126
Nayak BB, Mohanty BC, Singh SK (1996) Synthesis of silicon carbide from rice husk in a dc arc plasma reactor. J Am Ceram Soc 79(5):1197–1200
Pei L et al (2006) Preparation of silicon carbide nanotubes by hydrothermal method. J Appl Phys 99(11): 114306
Xie Z, Tao D, Wang J (2007) Synthesis of silicon carbide nanotubes by chemical vapor deposition. J Nanosci Nanotechnol 7(2):647–652
Tony V et al (2006) Characterization of silicon carbide nanotube synthesized using microwave heating
Conrads H, Schmidt M (2000) Plasma generation and plasma sources. Plasma Sources Sci Technol 9(4):441
Iwanowski R et al (1999) XPS and XRD study of crystalline 3C-SiC grown by sublimation method. J Alloy Compd 286(1–2):143–147
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The authors acknowledge the help and support received from their respective institutes.
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Sahu, R.K., Dash, T., Mukherjee, V., Pradhan, S.K., Nayak, B.B. (2021). Growth of Spheroidal Silicon Carbide by Arc Plasma Treatment. In: Ghosal, P., Carter, C.B., Vinothkumar, K.R., Sarkar, R. (eds) Applications of Microscopy in Materials and Life Sciences. Springer Proceedings in Materials, vol 11. Springer, Singapore. https://doi.org/10.1007/978-981-16-2982-2_8
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DOI: https://doi.org/10.1007/978-981-16-2982-2_8
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