Skip to main content

Investigation on Chemical Isolation and Characterization of Cellulose from Delonix regia Fruit Fibers

  • Conference paper
  • First Online:
Trends in Manufacturing and Engineering Management

Part of the book series: Lecture Notes in Mechanical Engineering ((LNME))

  • 1022 Accesses

Abstract

Lignocellulosic fibers have gained popularity among the research fraternity in recent years due to its abundance in nature, biodegradability, high specific strength, etc. Cellulose can be extracted from biomasses by various chemical and mechanical methods. In this paper, Delonix regia fruit fibers are presented as a new source of cellulose, and chemical methods are used for extraction of cellulose from it. Chemically treated and untreated fibers were characterized by X-ray diffraction (XRD) and thermogravimetric analysis (TGA) to understand the effect of chemical treatment and properties of the cellulose yield. The results obtained demonstrated that a high yield of cellulose is obtained by chemical extraction methods followed and validated the suitability of Delonix regia fruit fibers for various applications including biocomposites and bionanocomposites.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 129.00
Price excludes VAT (USA)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 169.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

References

  1. Krasznai DJ, Champagne Hartley R, Roy HM, Champagne P, Cunningham MF (2018) Compositional analysis of lignocellulosic biomass: conventional methodologies and future outlook. Crit Rev Biotechnol 38(2):199–217

    Google Scholar 

  2. Han JS (1997) Chemical composition of fibers, Chapter 5

    Google Scholar 

  3. Watkins D, Nuruddin M, Hosur M, Tcherbi-Narteh A, Jeelani S (2015) Extraction and characterization of lignin from different biomass resources. J Mater Res Technol 4(1):26–32

    Article  Google Scholar 

  4. Mohanty AK, Misra M, Hinrichsen G (2000) Biofibres, biodegradable polymers and biocomposites: an overview summary of contents 1. Introduction 2. Reinforcing biofibres 2.1 Chemical constituents and structural aspects 2.2 Properties of biofibres 2.3 Degradation properties of biofibres 2.4 Cost asp

    Google Scholar 

  5. Möller J (2014) Comparing methods for fibre determination in food and feed

    Google Scholar 

  6. Welker CM, Balasubramanian VK, Petti C, Rai KM, De Bolt S, Mendu V (2015) Engineering plant biomass lignin content and composition for biofuels and bioproducts. Energies 8(8):7654–7676

    Article  Google Scholar 

  7. Ayeni A, Adeeyo O, Oresegun O, Oladimeji T (2015) Compositional analysis of lignocellulosic materials: Evaluation of an economically viable method suitable for woody and non-woody biomass. Am J Eng Res 4(4):14–19

    Google Scholar 

  8. Senthilkumar N, Murugesan S, Sumathi R, Babu DS (2015) Tree species in India, vol 6, no 2, pp 25–28

    Google Scholar 

  9. Templeton DW, Scarlata CJ, Sluiter JB, Wolfrum EJ (2010) Compositional analysis of lignocellulosic feedstocks. 2. Method uncertainties. J Agric Food Chem 58(16):9054–9062

    Article  Google Scholar 

  10. Sluiter A et al (2011) Determination of structural carbohydrates and lignin in biomass determination of structural carbohydrates and lignin in biomass. Natl Renew Energy Lab 2011(July)

    Google Scholar 

  11. Giger-Reverdin S (1995) Review of the main methods of cell wall estimation: interest and limits for ruminants. Anim Feed Sci Technol 55(3–4):295–334

    Article  Google Scholar 

  12. Sun RC, Fang JM, Mott L, Bolton J (1999) Extraction and characterization of hemicelluloses and cellulose from oil palm trunk and empty fruit bunch fibres. J Wood Chem Technol 19(1):167–185

    Article  Google Scholar 

  13. Martins MA, Teixeira EM, Corrêa AC, Ferreira M, Mattoso LHC (2011) Extraction and characterization of cellulose whiskers from commercial cotton fibers. J Mater Sci 46(24):7858–7864

    Article  Google Scholar 

  14. Sun JX, Sun XF, Zhao H, Sun RC (2004) Isolation and characterization of cellulose from sugarcane bagasse. Polym Degrad Stab 84(2):331–339

    Article  MathSciNet  Google Scholar 

  15. Ibrahim MM, Agblevor FA, El-Zawawy WK (2010) solation and characterization of cellulose and lignin from steam-exploded lignocellulosic biomass. Biol Syst Eng 5:397–418

    Google Scholar 

  16. Singh S et al (2015) Comparison of different biomass pretreatment techniques and their impact on chemistry and structure. Front Energy Res 2(February):1–12

    Google Scholar 

  17. Suryanto H, Marsyahyo E, Irawan YS (2013) Morphology, structure, and mechanical properties of natural cellulose fiber from Mendong grass (Fimbristylis globulosa). J Nat Fibers (November 2014):37–41

    Google Scholar 

  18. Morán JI, Alvarez VA, Cyras VP, Vázquez A (2008) Extraction of cellulose and preparation of nanocellulose from sisal fibers. Cellulose 15(1):149–159

    Article  Google Scholar 

  19. Maheswari CU, Reddy KO, Muzenda E, Guduri BR, Rajulu AV (2012) Extraction and characterization of cellulose microfibrils from agricultural residue e Cocos nucifera L. Biomass Bioenerg 46:555–563

    Article  Google Scholar 

  20. Reddy KO et al (2018) Extraction and characterization of cellulose single fibers from native african napier grass. Carbohydr Polym 188:85–91

    Article  Google Scholar 

  21. Kalita RD, Nath Y, Ochubiojo ME, Buragohain AK (2013) Extraction and characterization of microcrystalline cellulose from fodder grass; Setaria glauca (L) P. Beauv, and its potential as a drug delivery vehicle for isoniazid, a first line antituberculosis drug. Colloids Surf B Biointerfaces 108:85–89

    Article  Google Scholar 

  22. Jahan MS, Saeed A, He Z, Ni Y (2011) Jute as raw material for the preparation of microcrystalline cellulose. Cellulose 18(2):451–459

    Article  Google Scholar 

  23. Nuruddin M et al (2011) Extraction and characterization of cellulose microfibrils from agricultural wastes in an integrated biorefinery initiative. Cellul Chem Technol 45(5–6):5–6

    Google Scholar 

  24. Ohwoavworhua F, Adelakun T, Okhamafe A (2009) Processing pharmaceutical grade microcrystalline cellulose from groundnut husk: extraction methods and characterization. Int J Green Pharm 3(2):97

    Article  Google Scholar 

Download references

Acknowledgements

I would like to thank Bombay Textile Research Association (BTRA), Mumbai (India), for providing necessary support and scientific help in compositional analysis. Also, I would like to thank National Institute of Technology, Raipur and Department of Physics, School of Sciences, Pt. Ravishankar Shukla University, Raipur for assisting in characterization.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Kalpit P. Kaurase .

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 2021 Springer Nature Singapore Pte Ltd.

About this paper

Check for updates. Verify currency and authenticity via CrossMark

Cite this paper

Kaurase, K.P., Singh, D. (2021). Investigation on Chemical Isolation and Characterization of Cellulose from Delonix regia Fruit Fibers. In: Vijayan, S., Subramanian, N., Sankaranarayanasamy, K. (eds) Trends in Manufacturing and Engineering Management. Lecture Notes in Mechanical Engineering. Springer, Singapore. https://doi.org/10.1007/978-981-15-4745-4_28

Download citation

  • DOI: https://doi.org/10.1007/978-981-15-4745-4_28

  • Published:

  • Publisher Name: Springer, Singapore

  • Print ISBN: 978-981-15-4744-7

  • Online ISBN: 978-981-15-4745-4

  • eBook Packages: EngineeringEngineering (R0)

Publish with us

Policies and ethics