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Preparation of iron aluminate (FeAl2O4) nanoparticles from FeAl2O4 hollow particles fabricated by using a spray pyrolysis process

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Abstract

Iron aluminate (FeAl2O4) hollow particles with a spinel structure were synthesized by using a spray pyrolysis process. FeAl2O4 hollow particles were formed at a reaction temperature of 900 °C at a flow rate of 40 L/min as a result of the rapid solvent evaporation and decomposition gases from the droplets in the spray solution prepared from metal salts and organic reagents. FeAl2O4 hollow particles were fabricated at a reaction temperature of 900 °C with a flow rate of 40 L/min. The FeAl2O4 hollow particles were heat treated for 3 hours at 600 °C in a 5% H2/Ar atmosphere to form the crystal particles. Subsequently, FeAl2O4 nanoparticles were fabricated from the FeAl2O4 hollow particles by using the wet milling process. After milling for 60 minutes, transmission electron microscopy revealed the FeAl2O4 particles to have a mean size of approximately 50 nm. The FeAl2O4 nanoparticles were fabricated successfully by using a two-step process, spray pyrolysis and wet milling.

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Authors and Affiliations

  1. Department of Material Science and Engineering, Pusan National University, Busan, 609-735, Korea

    Jaecheol Yun & Yangdo Kim

  2. Powder Technology Department, Korea Institute of Materials Science, Changwon, 642-831, Korea

    Dahee Park & Jung-Yeul Yun

Authors
  1. Jaecheol Yun
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  2. Yangdo Kim
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  3. Dahee Park
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  4. Jung-Yeul Yun
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Correspondence to Yangdo Kim or Jung-Yeul Yun.

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Yun, J., Kim, Y., Park, D. et al. Preparation of iron aluminate (FeAl2O4) nanoparticles from FeAl2O4 hollow particles fabricated by using a spray pyrolysis process. Journal of the Korean Physical Society 66, 1503–1507 (2015). https://doi.org/10.3938/jkps.66.1503

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  • DOI: https://doi.org/10.3938/jkps.66.1503

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