Skip to main content

Advertisement

Log in

Simultaneous Determination of Potassium and Nitrate Ions in Mouthwashes Using Sequential Injection Analysis with Potentiometric Detection

  • Notes
  • Published:
Analytical Sciences Aims and scope Submit manuscript

Abstract

Two methods for the determination of potassium nitrate in mouthwashes, used against dentin hypersensitivity, have been simultaneously implemented in an sequence injection analysis (SIA) system. In addition to in-line dilution of the samples, the equipment simultaneously detected potassium and nitrate using two tubular potentiometric detectors, selective to each ion, providing a real-time assessment of the quality of the results. Both determinations were shown to be precise and accurate and the obtained results do not statistically differ from those furnished by applying the AES and HPLC reference methods.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. M. Addy, Int. Dent. J., 2002, 52, 367.

    Article  Google Scholar 

  2. D. Hu, Y. P. Zhang, P. Chaknis, M. E. Petrone, A. R. Volpe, and W. De Vizio, J. Clin. Dent, 2004, 15, 6.

    PubMed  Google Scholar 

  3. J. C. Pereira, A. D. Segala, and D. G. Gillam, Dent. Mater., 2005, 21, 129.

    Article  CAS  Google Scholar 

  4. F. L. Pillon, I. G. Romani, and E. R. Schmidt, J. Periodontal., 2004, 75, 1461.

    Article  CAS  Google Scholar 

  5. R. Perez,-Olmos, P. Bezares, and J. Perez, II Fármaco, 2000, 5,99.

  6. J. M. Talamage and T. A. Biemer, J. Chromatogr, 1987, 410, 494.

    Article  Google Scholar 

  7. S. S. Chen, H. Lulla, F. J. Sena, and V. Reynoso, J. Chromatogr. Sci., 1985, 23, 355.

    Article  CAS  Google Scholar 

  8. H. Lulla, S. S. Chen, F. J. R. Sena, and D. Lab, J. Pharm. Sci., 1984, 74, 1004.

    Article  Google Scholar 

  9. C. C. Oliveira, R. P. Sartini, E. A. G. Zagatto, and J. L. F. C. Lima, Anal. Chim. Acta, 1997, 350, 31.

    Article  CAS  Google Scholar 

  10. R. Perez,-Olmos, J. C. Soto, N. Zarate, A. N. Araujo, and M. C. B. S. M. Montenegro, Anal. Chim. Acta, 2005, 554, 1.

    Article  CAS  Google Scholar 

  11. J. L. F. C. Lima, A. A. S. C. Machado, A. Florido, S. Alegret, and J. M. Paulis, Quim. Anal., 1985, 4, 145.

    CAS  Google Scholar 

  12. S. Alegret, J. Alonso, J. Bartroli, J. L. F. C. Lima, and A. A. S. C. Machado, Anal. Chim. Acta, 1984, 164, 147.

    Article  CAS  Google Scholar 

  13. S. Alegret, J. Alonso, J. Bartroli, A. A. S. C. Machado, J. L. F. C. Lima, and J. M. Paulis, Quim. Anal., 1987, 6, 278.

    CAS  Google Scholar 

  14. J. Alonso, J. Bartroli, J. L. F. C. Lima, and A. A. S. C. Machado, Anal. Chim. Acta, 1986, 179, 503.

    Article  CAS  Google Scholar 

  15. H. Kobler, in “High Performance Liquid Chromatography in Food Control and Research”, ed. R. Matisse and R. Wittkowski, 1993, Technomic Publishing Company, Lancaster.

  16. A. M. Pimenta, A. N. Araujo, and M. C. B. S. M. Montenegro, J. Pharm. Biomed. Anal, 2002, 30, 931.

    Article  CAS  Google Scholar 

  17. Analytical Methods Committee, Analyst, 1987, 112, 199.

    Article  Google Scholar 

  18. A. N. Araújo, R. C. C. Costa, J. L. F. C. Lima, and B. F. Reis, Anal. Chim. Acta, 1998, 358, 111.

    Article  Google Scholar 

  19. J. C. Miller and J. N. Miller, “Statistics for Analytical Chemistry”, 2nd ed., 1988, Ellis Horwood Ltd., Chichester, UK.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to R. Pérez-Olmos.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Zärate, N., Irázu, E., Araújo, A.N. et al. Simultaneous Determination of Potassium and Nitrate Ions in Mouthwashes Using Sequential Injection Analysis with Potentiometric Detection. ANAL. SCI. 24, 803–807 (2008). https://doi.org/10.2116/analsci.24.803

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.2116/analsci.24.803

Navigation