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Nanocrystal composites cement/BaCO3/Fe2O3 for improved X-ray shielding characteristics: Stability structural properties

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Abstract

Nanocrystal composites BaCO3/Fe2O3 were prepared using mechanical alloying for up to 56 h. From the analysis of X-ray diffraction (XRD) spectra, we choose three samples with the high concentration of BaFe12O19 phase for producing composites cement/BaCO3/Fe2O3. Refractive index (n), extinction coefficient (k), real (\(\epsilon\)1) and imaginary part (\(\epsilon\)2) dielectric function, and energy loss function (Im(−1/\(\epsilon\))) were determined from the quantitative analysis of Fourier transform infrared (FTIR) spectra using Kramers–Kronig relation. Radiation parameters were determined from X-ray mobile test data and then compared with theoretical calculation from XCOM database. We found the stable structural properties of all composites, indicated by similar crystallite size for before and after X-ray irradiation. The HVL for the highest energy is in the range of 0.280 to 0.291 cm indicated high potentials and effective alternative material for X-ray radiation shielding in future for development new radiology room.

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References

  1. E. Lacomme, M.I. Sayyed, H.A.A. Sidek, K.A. Matori, M.H.M. Zaid, Effect of bismuth and lithium substitution on radiation shielding properties of zinc borate glass system using Phy-X/PSD simulation. Results Phys. 20, 103768 (2021)

    Article  Google Scholar 

  2. H. Eskalen, Y. Kavun, S. Kerli, S. Eken, An investigation of radiation shielding properties of boron doped ZnO thin films. Opt. Mater. 105, 109871 (2020)

    Article  CAS  Google Scholar 

  3. T. Kaur, J. Sharma, T. Singh, Review on scope of metallic alloys in gamma rays shield designing. Prog. Nucl. Energy 113, 95–113 (2019)

    Article  CAS  Google Scholar 

  4. M.H.A. Mhareb, Y. Slimani, Y.S. Alajerami, M.I. Sayyed, E. Lacomme, M.A. Almessiere, Structural and radiation shielding properties of BaTiO3 ceramic with different concentrations of Bismuth and Ytterbium. Ceram. Int. 46(18), 28877–28886 (2020)

    Article  CAS  Google Scholar 

  5. I.S. Goncharov, N.G. Razamov, A.O. Silin, N.E. Ozerskoi, A.L. Shamshurin, A. Kim, Q.S. Wang, A.A. Popovich, Synthesis of Nb-based powder alloy by mechanical alloying and plasma spheroidization processes for additive manufacturing. Mater. Lett. 245, 188–191 (2019)

    Article  CAS  Google Scholar 

  6. Q.P. Zhang, D.M. Liang, W.F. Zhu, J.H. Liu, Y. Wu, D.G. Xu, X.Y. Bai, M. Wei, Y.L. Zhou, Fabrication of h-BN@PbWO4 with a facile sol-gel method towards enhanced photocatalytic and radiation shielding properties. J. Solid State Chem. 269, 594–599 (2019)

    Article  CAS  Google Scholar 

  7. R.M. Hamad, K.A. Ziq, R. Hamad, G. Saleh, A comprehensive ionizing radiation shielding study of FexSe0.5Te0.5 alloys with various iron concentrations. J. Alloys Compd. 858, 157636 (2021)

    Article  CAS  Google Scholar 

  8. A. Shayan, M. Abdellahi, F. Shahmohammadian, S. Jabbarzare, A. Khandan, H. Ghayour, Mechanochemically aided sintering process for the synthesis of barium ferrite: effect of aluminum substitution on microstructure, magnetic properties and microwave absorption. J. Alloy Compd. 708, 538–546 (2017)

    Article  CAS  Google Scholar 

  9. B.C. Reddy, H.C. Manjunatha, Y.S. Vidya, K.N. Sridhar, U.M. Pasha, L. Seenappa, C. Mahendrakumar, B. Sadashivamurthy, N. Dhananjaya, B.M. Sankarshan, S. Krishnaveni, K.V. Sathish, P.S.D. Gupta, Synthesis and characterization of multi functional nickel ferrite nano-particles for X-ray/gamma radiation shielding, display and antimicrobial applications. J. Phys. Chem. Solids 159, 110260 (2021)

    Article  CAS  Google Scholar 

  10. H. Fouzia, F. Mamoun, H. Naouel, A. Linda, M. Goussem, M. Said, A.S. Mohammed, M. Alex, A. Iost, S. Weiβ, A. Obrosov, The effect of milling time on the microstructure and mechanical properties of Ti-6Al-4Fe alloys. Mater. Today Commun. 27, 102428 (2021)

    Article  CAS  Google Scholar 

  11. Y. Xu, S. Zhou, B. Liao, S. Zhao, X. Dai, D. Chen, Effect of milling time on the microstructure and magnetic properties of amorphous Ti50Fe50 alloys prepared by mechanical alloying. J. Mater. Res. Technol. 8(5), 3929–3935 (2019)

    Article  CAS  Google Scholar 

  12. R. Verma, M.J. Rathod, R.K. Goyal, Effect of milling parameters on emi shielding of the pes/mwcnt nanocomposites. Mater. Today Proc. 43, 3169–3172 (2021)

    Article  CAS  Google Scholar 

  13. A.A. Othman, M.A. Osman, A.G. Abd-Elrahim, The effect of milling time on structural, optical and photoluminescence properties of ZnO nanocrystals. Optik 156, 161–168 (2018)

    Article  CAS  Google Scholar 

  14. M.A. Anugrah, S. Ilyas, D. Tahir, Gelatin/Poly (vinyl alcohol)/Inorganic filler composites for phantom breasts. Mater. Chem. Phys. 262, 124333 (2021)

    Article  CAS  Google Scholar 

  15. S. Suryani, H. Heryanto, R. Rusdaeni, A.N. Fahri, D. Tahir, Quantitative analysis of diffraction and infra-red spectra of composite cement/BaSO4/Fe3O4 for determining correlation between attenuation coefficient, structural and optical properties. Ceram. Int. 46(11), 18601–18607 (2020)

    Article  CAS  Google Scholar 

  16. A.H. Taqi, A.M. Ghalib, H.N. Mohammed, Shielding properties of Cu-Sn-Pb alloy by Geant4, XCOM and experimental data. Mater. Today Commun. 26(14), 101996 (2021)

    Article  CAS  Google Scholar 

  17. H. Akyildirim, E. Kavaz, F.I. El-Agawany, E. Yousef, Y.S. Rammah, Radiation shielding features of zirconolite silicate glasses using XCOM and FLUKA simulation code. J. Non-Cryst. Solids 545, 120245 (2020)

    Article  CAS  Google Scholar 

  18. W. Gallala, S. Hamdi, J. Martinez-Martinez, N. Almousa, G. Shkoukani, D. Moneghan, N. Fusi, M.E. Gaied, M. Montacer, M. Bourham, Effect of F-Ba and Pb-Zn tailing on the mechanical and radiation shielding properties of cement mortars. Constr. Build. Mater. 271, 121603 (2021)

    Article  CAS  Google Scholar 

  19. R.R. Mishra, A.K. Sharma, Microwave-material interaction phenomena: heating mechanisms, challenges and opportunities in material processing. Composites A 81, 78–97 (2016)

    Article  CAS  Google Scholar 

  20. R. Nazlan, I. Ismail, R.S. Aziz, Z. Abbas, I.R. Ibrahim, F.M. Idris, F.N. Shafiee, A.S. Aripin, N.A.N. Busra, Dependence of magnetic and microwave loss on evolving microstructure in yttrium iron garnet. J. Mater. Sci. 29, 8688–8700 (2018)

    CAS  Google Scholar 

  21. N. Al-Haj Husain, J. Camilleri, M. Özcan, Effect of polishing instruments and polishing regimens on surface topography and phase transformation of monolithic zirconia: an evaluation with XPS and XRD analysis. J. Mech. Behav. Biomed. Mater. 64, 104–112 (2016)

    Article  CAS  Google Scholar 

  22. P.S. Sundaram, T. Sangeetha, S. Rajakarthihan, R. Vijayalaksmi, A. Elangovan, G. Arivazhagan, XRD structural studies on cobalt doped zinc oxide nanoparticles synthesized by coprecipitation method: Williamson-Hall and size-strain plot approaches. Phys. B 595, 412342 (2020)

    Article  Google Scholar 

  23. P.L. Guzzo, F.B. de Barros Marinho, B.R. Soares, J.B. Santos, Evaluation of particle size reduction and agglomeration in dry grinding of natural quartz in a planetary ball mill. Powder Technol. 368, 149–159 (2020)

    Article  CAS  Google Scholar 

  24. X. Hu, P. Lu, Y. He, C. Wang, J. Chen, M. Fu, Anionic/cationic synergistic action of insulator BaCO3 enhanced the photocatalytic activities of graphitic carbon nitride. Appl. Surf. Sci. 528, 146924 (2020)

    Article  CAS  Google Scholar 

  25. C. Zeng, P. Li, H. Xu, Z. Xu, H. Li, Y. Zhang, Chemical synthesis of nanosized BaCO3 with a pillar-like morphology. Ceram. Int. 37(4), 1215–1218 (2011)

    Article  CAS  Google Scholar 

  26. S. Goel, A. Tyagi, A. Garg, S. Kumar, H.B. Baskey, R.K. Gupta, S. Tyagi, Microwave absorption study of composites based on CQD@BaTiO3 core shell and BaFe12O19 nanoparticles. J. Alloys Compd. 855, 157411 (2021)

    Article  CAS  Google Scholar 

  27. S. Anand, S. Pauline, V. Maria Vinosel, M. Asisi Janifer, Structural rietveld refinement and vibrational study of M-Type BaFe12O19 nanoparticles. Mater. Today Proc. 8, 476–483 (2019)

    Article  CAS  Google Scholar 

  28. D. Tahir, N.H. Sari, Stopping powers and inelastic mean free path of 200 eV-50 keV electrons in polymer PMMA, PE, and PVC. Appl. Radiat. Isotopes 95, 59–62 (2015)

    Article  CAS  Google Scholar 

  29. M.I. Sayyed, H.O. Tekin, O. Kılıcoglu, O. Agar, M.H.M. Zaid, Shielding features of concrete types containing sepiolite mineral: comprehensive study on experimental XCOM and MCNPX results. Results Phys. 11, 40–45 (2018)

    Article  Google Scholar 

  30. M. Eshghi, Investigation of radiation protection features of the TeO2–B2O3–Bi2O3–Na2O–NdCl3 glass systems. J. Mater. 31, 16479–16497 (2020)

    CAS  Google Scholar 

  31. P. Sopapan, J. Laopaiboon, O. Jaiboon, C. Yenchai, R. Laopaiboon, Feasibility study of recycled CRT glass on elastic and radiation shielding properties used as x-ray and gamma-ray shielding materials. Prog. Nucl. Energy 119, 103149 (2020)

    Article  CAS  Google Scholar 

  32. C.G. Hernandez-Murillo, J.R. Molina Contreras, L.A. Escalera-Velasco, H.A. de Leon-Martínez, J.A. Rodriguez-Rodriguez, H.R. Vega-Carrillo, X-ray and gamma ray shielding behavior of concrete blocks. Nucl. Eng. Technol. 52(8), 1792–1797 (2020)

    Article  CAS  Google Scholar 

  33. H.H. Nguyen, W.H. Jeong, T.L. Phan, B.W. Lee, D.S. Yang, N. Tran, N.T. Dang, Coexistence of Zn and Fe ions influenced magnetic and microwave shielding properties of Zn-doped SrFe12O19 ferrites. J. Magn. Magn. Mater. 537, 168195 (2021)

    Article  CAS  Google Scholar 

  34. S. Aly, H.A. El-Boraey, Effect of gamma irradiation on spectral, XRD, SEM, DNA binding, molecular modling and antibacterial property of some (Z)–N-(furan-2-yl)methylene)-2-(phenylamino)acetohydrazide metal(II) complexes. J. Mol. Struct. 1185, 323–332 (2019)

    Article  CAS  Google Scholar 

  35. B. Abdullah, D. Tahir, Quantitative analysis of X-Ray diffraction spectra for determine structural properties and deformation energy of Al, Cu and Si. IOP Conf. Ser. 1317, 012052 (2019)

    Article  Google Scholar 

  36. R. Zamiri, H.M. Chenari, H.F. Moafi, M. Shabani, S.A. Salehizadeh, A. Rebelo, J.S. Kumar, M.P.F. Graca, M.J. Soares, J.M.F. Ferreira, Ba-doped ZnO nanostructure: X-ray line analysis and optical properties in visible and low frequency infrared. Ceram. Int. 42(11), 12860–12867 (2016)

    Article  CAS  Google Scholar 

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Acknowledgments

This work was supported by the PT (Penelitian Terapan) funded by the Indonesia Government (DIKTI/BRIN) 2021 Grant: 752/UN4.22/PT.01.03/2022.

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AA: Writing—original draft. RR, MA, and HH: Software, Validation Writing—original draft. DT: Writing—original draft, Editing, review, and finalization.

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Correspondence to Dahlang Tahir.

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Ardiansyah, A., Rahmat, R., Azlan, M. et al. Nanocrystal composites cement/BaCO3/Fe2O3 for improved X-ray shielding characteristics: Stability structural properties. Journal of Materials Research 37, 4114–4123 (2022). https://doi.org/10.1557/s43578-022-00775-z

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