Abstract
A nanomaterial that attracts the attention in a variety of research areas is multiwall carbon nanotubes (MWCNTs), due to their good mechanical proprieties, and high electrical and thermal conductivity. For this reason, the preparation of three-dimensional (3D) structures from them draws interest because it opens new horizons to produce materials with novel properties and useful applications. In this investigation the synthesis of 3D nanotube carbon (nanoforest type) functionalized with nanoparticles of silver, aluminum, and iron was studied. A 3D structure was produced in the form of aligned microchannels. The functionalization of carbon nanotubes with nanoparticles of silver, aluminum or iron during the synthesis process of carbon nanotubes, was carried out through spray-pyrolysis with different synthesis time and solution concentration. The results were characterized through microscopy SEM, TEM and Raman’s spectroscopy.
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H. Butt, R. Rajesekharan, Q. Dai, S. Sarfraz, V. Kumar R., G .A. J. Amaratunga, T. D. Wilkinson, Cylindrical Fresnel lenses based on carbon nanotube forests, Applied Physics Letters, 2012, 101(24), Article number 243116.
T. Saleh, M. Vahdani Moghaddam, M. Sultan Mohamed Ali, M. Dahmardeh, C. Alden Foell, A. Nojeh, K. Takahata Transforming carbon nanotube forest from darkest absorber to reflective mirror, Appl. Phys. Lett., 2012, 101, 061913.
H. Chen, A. Roy, J.-B. Baek, L. Zhu, J. Qu, L. Dai, Controlled growth and modification of vertically-aligned carbon nanotubes for multifunctional applications, Mater. Sci. Eng. R: Reports, 2010, 70, 63–91.
N. Hayashi, S.-I. Honda, K. Tsui, K.-Y. Lee, T. Ikuno, K. Fujimoto, S. Ohkura, M. Katayama, K. Oura, T. Hirao. Highly aligned carbon nanotube arrays fabricated by bias sputtering, Appl. Surf. Sci. 2003, 212–213 393–396.
C. Daraio, V. F. Nesterenko, S. Jin, Impact response by a foamlike forest of coiled carbon nanotubes, J.Appl. Phys. 2006, 100, 064309, 4 pp.
Y. Taki, M. Kikuchi, K. Shinohara, A. Tanaka, Selective Growth of Vertically Aligned Single-, Double-, and Triple-Walled Carbon Nanotubes by Radiation-Heated Chemical Vapor Deposition, Jpn. J. Appl. Phys. 2008, 47, 721–724.
A. M. Cassell, M. Meyyappan, J. Han, Multilayer Film Assembly of Carbon Nanotubes, J. Nanopart. Res. 2000, 2(4), 387–389.
Q. Zhang, W. Zhou,W. Qian, R. Xiang, J. Huang, D. Wang, F. Wei, Synchronous Growth of Vertically Aligned Carbon Nanotubes with Pristine Stress in the Heterogeneous Catalysis Process, J. Phys. Chem. C, 2007, 111, 14638–14643.
X. Li, A. Cao, Y. J. Jung, R. Vajtai, P. M. Ajayan, Bottom-Up Growth of Carbon Nanotube Multilayers: Unprecedented Growth, Nano Lett. 2005, 5, 1997–2000.
S. Huang, L. Dai, A. W. H. Mau, Nanotube “crop circles”, J. Mater. Chem. 1999, 9, 1221–1222.
C. K. Tan, K. P. Loh, T. T. L. John, Direct amperometric detection of glucose on a multiple-branching carbon nanotube forest, Analyst, 2008, 133, 448–451.
S. Li, H. Li, X. Wang, Y. Song, Y. Liu, L. Jiang, D. Zhu, Super-Hydrophobicity of Large-Area Honeycomb-Like Aligned Carbon Nanotubes, J. Phys. Chem. B, 2002, 106(36) 9274–9276.
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Kharissova, O.V., Garcia, B.O., Guillén, P.Y.A. et al. Synthesis and characterization of 3D carbon nanotubes. MRS Advances 3, 103–108 (2018). https://doi.org/10.1557/adv.2018.181
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DOI: https://doi.org/10.1557/adv.2018.181