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Preparation of γ–Fe2O3 nanoparticles from a nonaqueous precursor

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Abstract

Nanosized particles of γ–Fe2O3 were prepared by heat treatment of the precipitates, obtained from a homogeneous solution of stearic acid and hydrated iron(III) nitrate. The compositional and thermal characteristics of the precipitates were studied with the aid of infrared spectroscopy and differential scanning calorimetry. The x-ray diffraction and small-angle x-ray scattering investigation shows that γ–Fe2O3 nanoparticles with narrow size distribution can be prepared successfully by this route.

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References

  1. M. P. Morales, M. Andres-Verges, S. Veintemillas-Verdaguer, M.I .Montero, and C. J. Serna, J. Magn. Magn. Mater. 203,146 (1999).

    Article  CAS  Google Scholar 

  2. J. L. Dormann, P. Deb, and A. Basumallick, J. Magn. Magn. Mater. 203, 23 (1999).

    Article  CAS  Google Scholar 

  3. S. Grimm, M. Schultz, S. Barth, and R. Muller, J. Mater. Sci. 32, 1083 (1997).

    Article  CAS  Google Scholar 

  4. R. P. Cowbern, A. M. Moulinand, and M. E. Welland, Appl. Phys. Lett. 71, 2202 (1997).

    Article  CAS  Google Scholar 

  5. T. Ishikawa, T. Takeda, and K. Kandori, J. Mater. Sci. 27, 4531 (1992).

    Article  Google Scholar 

  6. O. V. Lounansmaa, Phys. Scr. 66, 70 (1996).

    Article  CAS  Google Scholar 

  7. S. C. Davies, C. Ni, J. Fardyu, and D. Rassi, J. Med. Eng. Technol. 18, 127 (1994).

    Article  Google Scholar 

  8. O. Glatter and O. Kratky, Small Angle X-ray Scattering (Academic Press, London, United Kingdom, 1982).

    Article  CAS  Google Scholar 

  9. A. Guiner, G. Fournet, B. C. Walker, and L.K. Yudowith Small Angle Scattering of X-Rays (Wiley, New York, 1955).

    Google Scholar 

  10. M. K. Wilson, in Determination of organic structures by physical methods, edited by F.C. Nachod and W.D. Phillips (Academic Press, New York, 1962), Vol. 2, Chapter 3, p. 181.

    Google Scholar 

  11. J.R. Ryder Application of Absorption Spectroscopy of Organic Compounds (Prentice Hall of India, New Delhi, India, 1987), p.22.

    Google Scholar 

  12. A. Miller, Arzeinmitel Forsch. 17, 921 (1967).

    Google Scholar 

  13. M. P. Morales, C. Percharroman, T. Gonzales Carreno, and C.J. Serna, J. Solid State Chem. 108, 158 (1994).

    Google Scholar 

  14. N. Irving Sax and R. J. Lewis, Sr., Hawley’s Condensed Chemical Dictionary, 11th ed. (CBS publication and distributors, New Delhi, India, 1990), p. 1091.

    Article  CAS  Google Scholar 

  15. S. Enzo, G. Fagherazzi, A. Benedetti, and S. Polizzi, J. Appl. Crystallogr. 21, 536 (1988).

    Google Scholar 

  16. Th. H. DE Keijser, E. Mittemeijer, and H.C. F. Rozenda, J. Appl. Crystallogr. 16, 309 (1983).

    Article  Google Scholar 

  17. D. Sen, P. Deb, S. Mazumder, and A. Basumallick, Mater. Res. Bull. 35, 1243 (2000).

    Article  Google Scholar 

  18. C.S. Hwang, J. Mater . Sci. Eng. B 56, 178 (1998).

    Article  Google Scholar 

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Deb, P., Basumallick, A. Preparation of γ–Fe2O3 nanoparticles from a nonaqueous precursor. Journal of Materials Research 16, 3471–3475 (2001). https://doi.org/10.1557/JMR.2001.0477

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  • DOI: https://doi.org/10.1557/JMR.2001.0477

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