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Face-centered-cubic titanium: An artifact in titanium/aluminum multilayers

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Abstract

The present investigation is the first comprehensive comparative study of x-ray diffraction (XRD) and transmission electron microscopy (TEM) results to address the important issue of fcc Ti formation in nanoscale multilayers. Ti/Al multilayers with 7.2 and 5.2 nm composition modulation wavelengths were studied by reflection and transmission XRD as well as transmission electron diffraction (ED), high-resolution TEM, and energy-filtered TEM. Previous reports have claimed deposition of fcc Ti in multilayer systems. Our results demonstrate that the Ti in Ti/Al multilayers deposits in the hcp form and that fcc Ti is merely an artifact of producing specimens for cross-sectional TEM.

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Bonevich, J., van Heerden, D. & Josell, D. Face-centered-cubic titanium: An artifact in titanium/aluminum multilayers. Journal of Materials Research 14, 1977–1981 (1999). https://doi.org/10.1557/JMR.1999.0266

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  • DOI: https://doi.org/10.1557/JMR.1999.0266

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