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Determination of Apigenin by LC with Electrochemical Detection

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Abstract

Sodium dodecylsulfonate (SDS) was used as a sensitizer for the determination of apigenin by LC with electrochemical detection (ECD). It was found that when SDS was added to the mobile phase, the limit of detection of apigenin obtained with ECD was 3.5 × 10−2 μg mL−1. The method was successfully applied to the analysis of apigenin in four samples (Scutellaria barbata, Buddleja officinalis, Carthamus tinctorius L. and onion), and was found to be especially useful in the case of small amounts of sample.

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References

  1. Liu C (2005) Foreign Med Sci (Neurol & Neurosurg) 32:274–267

    Google Scholar 

  2. Sun B, Qu WQ, Zhang XL (2004) J Chin Med Mat 27:531–534

    Google Scholar 

  3. Singh VPJ, Selvendiran K, Banu SM, Padmavathi R, Sakthisekaran D (2004) Phytomed 11:309–314

    Article  CAS  Google Scholar 

  4. Ricupero DA, Poliks CF, Rishikof DC, Ping KP, Goldstein RH (2001) FEBS Letter 506:15–21

    Article  CAS  Google Scholar 

  5. Verbeek R, Plomp AC, Tol EAFV, Noort JMV (2004) Biochem Pharmacol 68:621–629

    Article  CAS  Google Scholar 

  6. Losi G, Puia G, Garzon G, Vuono MCD, Baraldi M (2004) Eur J Pharmacol 502:41–46

    Article  CAS  Google Scholar 

  7. Rithidech KN, Tungjai M, Whorton EB (2005) Toxicol Environ Mutagen 585:96–104

    Article  CAS  Google Scholar 

  8. Noel S, Kasinathan M, Rath SK (2006) Toxicol Vitro 20:1168–1172

    Article  CAS  Google Scholar 

  9. Bektic J, Guggenberger R, Spengler B, Christoffel V, Pelzer A, Berger AP, Ramoner R, Bartsch G, Klocker H (2006) Maturitas 55:S37–S46

    Article  CAS  Google Scholar 

  10. Maruta A, Enaka K, Umeda M (1979) Gann 70:273–276

    CAS  Google Scholar 

  11. Stoewsand GS, Anderson JL, Boyd JN, Hrazdina G, Babish JG, Walsh KM, Losco P (1984) J Toxicol Environ Health 14:105–114

    Article  CAS  Google Scholar 

  12. Liu ZM, Huang YN (2006) J Southwest Chin Norm Univ (Nat Sci) 31:89–92

    CAS  Google Scholar 

  13. Xu XQ, Yu LS, Chen GN (2006) J Pharm Biomed Anal 41:493–499

    Article  CAS  Google Scholar 

  14. Fu L, Chu QC, Huang BK, Zheng HC, Ye JN (2005) Chin J Anal Chem 33:161–164

    CAS  Google Scholar 

  15. Lü YQ, Wu CH, Yuan ZB, (2005) Chin J Anal Chem 33:805–807

    Google Scholar 

  16. Sudjaroen Y, Haubner R, Würtele G, Hull WE, Erben G, Spiegelhalder B, Changbumrung S, Bartsch H, Owen RW (2005) Food Chem Toxicol 43:1673–1682

    Article  CAS  Google Scholar 

  17. Luo MN, Zhao L, Liu X, Jiang SX (2006) Chin J Pharm Anal 26:1773–1776

    CAS  Google Scholar 

  18. Qiao CF, Han QB, Song JZ, Mo SF, Dai P, Xu HX (2006) Chin Phatm J 41:1342–1344

    CAS  Google Scholar 

  19. Liu GT (2004) Chem & Bioeng 6:51–53

    CAS  Google Scholar 

  20. Scalia S, Giuffreda L, Pallado P (1999) J Pharm Biomed Anal 21:549–558

    Article  CAS  Google Scholar 

  21. Volpi N, Bergonzini G (2006) J Pharm Biomed Anal 42:354–361

    Article  CAS  Google Scholar 

  22. Sladkovsky R, Solich P, Urbanek M (2004) J Chromatogr A 1040:179–184

    Article  CAS  Google Scholar 

  23. Spadaro A, Bousquet E, Santagati NA, Vittorio F, Ronsisvalle G (2005) Chromatographia 62:11–15

    Article  CAS  Google Scholar 

  24. Plavsic M, Krznaric D, Cosovic B (1994) Electroanalysis 6:469–474

    Article  CAS  Google Scholar 

  25. Dang XP, Chen WH, Hh SS (2004) J Wuhan Univ (Nat Sci Ed) 50:141–145

    CAS  Google Scholar 

  26. Xu DK, Lin H, Chen HY (1997) Anal Chim Acta 439:215–219

    Article  Google Scholar 

  27. Jiang SM, Hu YZ, Fu CG (2004) Chem Anal Mete 13:15–17

    CAS  Google Scholar 

Download references

Acknowledgments

The authors gratefully acknowledge the financial support of this project by the National Science Foundation of China (No. 20675062).

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Correspondence to Jian-Bin Zheng.

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Liu, XL., Zhang, HF., Qiao, GJ. et al. Determination of Apigenin by LC with Electrochemical Detection. Chroma 68, 147–150 (2008). https://doi.org/10.1365/s10337-008-0646-y

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  • DOI: https://doi.org/10.1365/s10337-008-0646-y

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