Abstract
2,2′: 5′,2″-Terthiophene derivative containing benzo-18-crown-6 fragments linked through ethene spacers was synthesized, and its complexation with octane-1,8-diaminium diperchlorate in acetonitrile was studied by spectrophotometric titration, 1H NMR, and mass spectrometry. The 1: 1 stoichiometry of the complex was confirmed by mass spectrometry, and its structure was proposed on the basis of the 1H NMR data.
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Original Russian Text © E.V. Lukovskaya, A.A. Kosmacheva, O.A. Fedorova, A.A. Bobyleva, A.V. Dolganov, N.E. Shepel’, Yu.V. Fedorov, V.V. Novikov, A.V. Anisimov, 2014, published in Zhurnal Organicheskoi Khimii, 2014, Vol. 50, No. 4, pp. 563–569.
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Lukovskaya, E.V., Kosmacheva, A.A., Fedorova, O.A. et al. Synthesis of chromophoric crown-containing styryl derivative of terthiophene and its complexation with octane-1,8-diaminium diperchlorate. Russ J Org Chem 50, 552–558 (2014). https://doi.org/10.1134/S1070428014040198
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DOI: https://doi.org/10.1134/S1070428014040198