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Intramolecular cyclization of dialkyl[2-(5-chloro-2-hydroxyphenyl)-2-phenylethenyl]phosphine oxides by the action of thionyl chloride

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Abstract

An efficient procedure has been proposed for the synthesis of quasiphosphonium salts, 2,2-dialkyl-6-chloro-4-phenyl-2H-1,2-benzoxaphosphinin-2-onium chlorides, via cyclization of dialkyl[2-(5-chloro-2-hydroxyphenyl)-2-phenylethenyl]phosphine oxides under the action of thionyl chloride.

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Authors and Affiliations

  1. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, ul. Arbuzova 8, Kazan, 420088, Tatarstan, Russia

    D. A. Tatarinov, D. M. Kuznetsov & V. F. Mironov

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  1. D. A. Tatarinov
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  2. D. M. Kuznetsov
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  3. V. F. Mironov
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Correspondence to D. A. Tatarinov.

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Original Russian Text © D.A. Tatarinov, D.M. Kuznetsov, V.F. Mironov, 2014, published in Zhurnal Organicheskoi Khimii, 2014, Vol. 50, No. 4, pp. 555–557.

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Tatarinov, D.A., Kuznetsov, D.M. & Mironov, V.F. Intramolecular cyclization of dialkyl[2-(5-chloro-2-hydroxyphenyl)-2-phenylethenyl]phosphine oxides by the action of thionyl chloride. Russ J Org Chem 50, 544–546 (2014). https://doi.org/10.1134/S1070428014040174

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  • DOI: https://doi.org/10.1134/S1070428014040174

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