Abstract
2,3-Bis[allylsulfanyl(amino)methylidene]succinonitrile was synthesized by alkylation of cyanothioacetamide with allyl bromide in DMF in the presence of aqueous potassium hydroxide, and its molecular and crystal structures were studied by X-ray analysis.
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Howard, E.G., US Patent no. 2733260, 1956; Chem. Abstr., 1956, vol. 50, p. 12 104.
Abdel-Galil, F.M., Sherif, Sh.M., and Elnagdi, M.H., Heterocycles, 1986, vol. 24, p. 2023; Elnagdi, M.H., Sherif, Sh.M., and Mohareb, R.M., Heterocycles, 1987, vol. 26, p. 497; Riad, B.Y., Negm, A.M., Abdou, S.E., and Daboun, H.A., Heterocycles, 1987, vol. 26, p. 205; Litvinov, V.P., Promonekov, V.K., Sharanin, Yu.A., and Shestopalov, A.M., Itogi Nauki Tekh., Ser. Org. Khim., 1989, vol. 17, p. 72; Sharanin, Yu.A., Promonenkov, V.K., and Litvinov, V.P., Itogi Nauki Tekh., Ser. Org. Khim., 1991, vol. 20, p. 1; Sausin’sh, A.E. and Dubur, G.Ya., Khim. Geterotsikl. Soedin., 1992, p. 435; Ozols, Ya., Vigante, B., and Duburs, G., Khim. Geterotsikl. Soedin., 1994, p. 1603; Dyachenko, V.D., Doctoral (Chem.) Dissertation, Moscow, 1998; Jagodzinski, T.S., Chem. Rev., 2003, vol. 103, p. 197.
Dyachenko, V.D., Nesterov, V.N., Promonenkov, V.K., Sharanin, Yu.A., Shklover, V.E., and Struchkov, Yu.T., Abstracts of Papers, Vsesoyuznaya konferentsiya “Khimiya i tekhnologiya piridinsoderzhashchikh pestitsidov” (All-Union Conf. “Chemistry and Technology of Pyridine-Containing Pesticides”), Chernogolovka, 1988, p. 120.
Schafer, H. and Gewald, K., J. Prakt. Chem., 1974, vol. 316, p. 684.
Abdel, A.M.A., Daboun, H.A., and Abdel, G.S.M., J. Serb. Chem. Soc., 1990, vol. 55, p. 79.
Volovenko, Yu.M., Khilya, O.V., Volovnenko, T.A., and Shokol, T.V., Khim. Geterotsikl. Soedin., 2002, p. 350.
Dyachenko, V.D., Abstracts of Papers, XIX Ukrains’ka konferentsiya z organichnoi khimii (XIXth Ukrainian Conf. on Organic Chemistry), L’viv, 2001, p. 354.
Hobbs, F.W., US Patent no. 6703420, 2004; Ref. Zh., Khim., 2004, no. 04.21-19O50P.
Alder, R.W., Goode, N.C., King, T.J., Mellor, J.M., and Miller, B.W., J. Chem. Soc., Chem. Commun., 1976, p. 173.
Burke-Laing, M. and Laing, M., Acta Crystallogr., Sect. B, 1976, vol. 32, p. 3216.
Kitaigorodsky, A.I., Molecular Crystals and Molecules, New York: Academic, 1973, p. 431.
Allen, F.H., Kennard, O., Watson, D.G., Brammer, L., Orpen, A.G., and Taylor, R., J. Chem. Soc., Perkin Trans. 2, 1987, p. S1.
Kuleshova, L.N. and Zorkii, P.M., Acta Crystallogr., Sect. B, 1981, vol. 37, p. 1363.
Watkin, D.J., Prout, C.K., Carruthers, J.R., and Betteridge, P.W., CRYSTALS. Issue 10, Chemical Crystallography Laboratory, Oxford Univ., 1996.
Carruthers, J.R. and Watkin, D.J., Acta Crystallogr., Sect. A, 1979, vol. 35, p. 698.
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Original Russian Text © V.D. Dyachenko, A.N. Chernega, 2006, published in Zhurnal Organicheskoi Khimii, 2006, Vol. 42, No. 7, pp. 967–969.
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Dyachenko, V.D., Chernega, A.N. Synthesis of 2,3-bis[allylsulfanyl(amino)methylidene]succinonitrile and its molecular and crystal structure. Russ J Org Chem 42, 945–948 (2006). https://doi.org/10.1134/S1070428006070013
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DOI: https://doi.org/10.1134/S1070428006070013