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Synthesis of ZSM-12 Zeolites with New Templates Based on Salts of Ethanolamines

  • Inorganic Synthesis and Industrial Inorganic Chemistry
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Abstract

New class of templates, ethanolamine salts, was used to synthesize zeolites with the ZSM-12 structure. The materials obtained were characterized by methods of powder X-ray diffraction, scanning electron microscopy, IR spectroscopy, low-temperature adsorption–desorption of nitrogen, and elemental analysis. It was shown that, with these templates, it is possible to obtain crystallites with well formed acicular shape, hexagonal morphology, large surface area, and narrow pore size distribution.

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References

  1. US Patent 3 832 449 (publ. 1974).

  2. Dimitrov, L., Mihaylov, M., Hadjiivanov, K., Mavrodinova, V., Microporous Mesoporous Mater., Elsevier Inc., 2011, vol. 143, nos. 2–3, pp. 291–301.

    Article  CAS  Google Scholar 

  3. Jegatheeswaran, S., Cheng, C.M., and Cheng, C.H., Microporous Mesoporous Mater., Elsevier Inc., 2015, vol. 201, no. C, pp. 24–34.

    Article  CAS  Google Scholar 

  4. Li, J., Lou, L.-L., Xu, C., and Liu, S., Catal. Commun., Elsevier B, V, 2014, vol. 50, pp. 97–100.

    CAS  Google Scholar 

  5. Sanhoob, M.A., Muraza, O., Taniguchi, T., Tago, T., Watanabe, G., and Masuda, T., Microporous Mesoporous Mater., 2014, vol. 194, pp. 31–37.

    Article  CAS  Google Scholar 

  6. Masoumifard, N., Kaliaguine, S., and Kleitz, F., Microporous Mesoporous Mater., 2016, vol. 227, pp. 258–271.

    Article  CAS  Google Scholar 

  7. Chaves, T.F., Carvalho, K.T.G., Urquieta-González, E.A., and Cardozo, D., Catal. Lett., 2016, vol. 146, no. 10, pp. 2200–2213.

    Article  CAS  Google Scholar 

  8. Sanhoob, M.A., Muraza, O., Al-Mutairi, E.M., and Ullah, N., Adv. Powder Technol. Soc., Powder Technol. Japan, 2015, vol. 26, no. 1, pp. 188–192.

    Article  CAS  Google Scholar 

  9. Kinski, I., Daniels, P., Deroche, C., Marler, B., and Gies, H., Microporous Mesoporous Mater., 2002, vol. 56, no. 1, pp. 11–25.

    Article  CAS  Google Scholar 

  10. US Patent 4 452 769 (publ. 1983).

  11. Zhu, H.-B., Xia, Q.-H., Guo, X.-T., Su, K.-X., Hu, D., Ma, X., Zeng, D., and Deng, F., Mater. Lett., 2006, vol. 60, nos. 17–18, pp. 2161–2166.

    Article  CAS  Google Scholar 

  12. Wu, W., Wu, W., Kikhtyanin, O.V., Li, L., Toktarev, A.V., Ayupov, A.B., Khabibulin, J.F., Echevsky, G.V., and Huang, J., Appl. Catal. A, 2010, vol. 375, no. 2, pp. 279–288.

    Article  CAS  Google Scholar 

  13. Carvalho, K.T.G. and Urquieta-Gonzalez, E.A., Catal. Today, 2015, vol. 243, no. 1, pp. 92–102.

    Article  CAS  Google Scholar 

  14. Chiche, B.H., Dutartre, R., Di Renzo, F., and Fajula, F., Catal. Lett., 1995, vol. 31, no. 4, pp. 359–366.

    Article  CAS  Google Scholar 

  15. Xia, Q.-H., Shen, S.-C., Song, J., Kawi, S., and Hidajat, K., J. Catal., 2003, vol. 219, no. 1, pp. 74–84.

    Article  CAS  Google Scholar 

  16. Ritsch, S., Ohnishi, N., Ohsuna, T., Hiraga, K., Terasaki, O., Kubota, Y., and Sugi, Y., Chem. Mater., 1998, vol. 10, no. 12, pp. 3958–3965.

    Article  CAS  Google Scholar 

  17. Zhao, Y., Zhang, H., Wang, P., Xue, F., Ye, Z., Zhang, Y., and Tang, Y., Chem. Mater., 2017, vol. 29, no. 8, pp. 3387–3396.

    Article  CAS  Google Scholar 

  18. Mehla, S., Krishnamurthy, K.R., Viswanathan, B., John, M., Niwate, Y., Kishore Kumar, S.A., Pai, S.M., and Newalkarb, B.L., Microporous Mesoporous Mater., Elsevier Inc., 2013, vol. 177, pp. 120–126.

    Article  CAS  Google Scholar 

  19. Souza, M.J.B., Silva, A.O.S., Garrido Pedrosa, A.M., and Araujo, A.S., React. Kinet. Catal. Lett., 2005, vol. 84, no. 2, pp. 287–293.

    Article  CAS  Google Scholar 

  20. Araujo, A.S., Silva, A.O.S., Souza, M.J.B., Coutinho, A.C.S.L.S., Aquino, J.M.F.B., Moura, J.A., and Pedrosa, A.M.G., Adsorption, 2005, vol. 11, no. 2. Spec. Issue, pp. 159–165.

    Article  CAS  Google Scholar 

  21. Gopal, S., Yoo, K., and Smirniotis, P.G., Microporous Mesoporous Mater., 2001, vol. 49, nos. 1–3, pp. 149–156.

    Article  CAS  Google Scholar 

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Authors and Affiliations

  1. Lomonosov Moscow State University, Moscow, 119991, Russia

    D. E. Tsaplin, D. A. Makeeva, L. A. Kulikov, A. L. Maksimov & E. A. Karakhanov

  2. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Moscow, 119991, Russia

    L. A. Kulikov & A. L. Maksimov

Authors
  1. D. E. Tsaplin
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  2. D. A. Makeeva
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  3. L. A. Kulikov
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  4. A. L. Maksimov
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  5. E. A. Karakhanov
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Corresponding author

Correspondence to L. A. Kulikov.

Additional information

Original Russian Text © D.E. Tsaplin, D.A. Makeeva, L.A. Kulikov A.L. Maksimov, E.A. Karakhanova, 2018, published in Zhurnal Prikladnoi Khimii, 2018, Vol. 91, No. 12, pp. 1729−1734.

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Tsaplin, D.E., Makeeva, D.A., Kulikov, L.A. et al. Synthesis of ZSM-12 Zeolites with New Templates Based on Salts of Ethanolamines. Russ J Appl Chem 91, 1957–1962 (2018). https://doi.org/10.1134/S1070427218120066

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  • DOI: https://doi.org/10.1134/S1070427218120066

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