Abstract
Method for microwave liquid-phase synthesis of hydroxyapatite samples was developed. The composition of the synthesis products obtained and natural hydroxyapatite was studied by X-ray phase and X-ray fluorescence microanalysis. IR spectra were measured and the dispersity of hydroxyapatite powders obtained, their solubility in water at 20°C, and structural parameters were determined in comparison with natural hydroxyapatite and that produced by the common (“classical”) liquid-phase technique. The microwave-synthesized hydroxyapatite compares well in its properties with the biological and “classical” hydroxyapatites.
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Solunin, V.L., Shapovalov, A.B., and Vlasova, E.B., Steklo Keram., 2010, no. 12, p. 27.
Barinov, S.M. and Komlev, V.S., Biokeramika na osnove fosfatov kal’tsiya (Bioceramics Based on Calcium Phosphates), Moscow: Nauka, 2005.
Mikheev, A.N. and Pankrushina, N.A., Nauka Sibiri, 2010, no. 21, p. 9.
Berdonosov, S.S., Soros. Obrazovat. Zh., 2001, vol. 7, no. 1, p. 32.
Jarcho, M. and Bolen, C.H., J. Mater. Sci., 1976, no. 11, p. 2027.
Petrovskaya, T.S., Rasskazova, L.A., Korotchenko, N.M., et al., Izv. Tomsk Politekhn. Univ., 2010, vol. 317, no. 3, p. 86.
Kumok, V.N. and Skorik, N.A., Laboratornye raboty po khimii kompleksnykh soedinenii (Laboratory Works on Chemistry of Complex Compounds), Tomsk: Tomsk Gos. Univ., 1983.
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Original Russian Text © L.A. Rasskazova, N.M. Korotchenko, G.M. Zeer, 2013, published in Zhurnal Prikladnoi Khimii, 2013, Vol. 86, No. 5, pp. 744–748.
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Rasskazova, L.A., Korotchenko, N.M. & Zeer, G.M. Microwave synthesis of hydroxyapatite and physicochemical study of its properties. Russ J Appl Chem 86, 691–695 (2013). https://doi.org/10.1134/S1070427213050145
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DOI: https://doi.org/10.1134/S1070427213050145