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Synthesis and Characterization of Water-Soluble Arabinogalactan-Stabilized Bismuth Telluride Nanoparticles

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Abstract

Water-soluble nanocomposites consisting of arabinogalactan (AG)-stabilized Bi2Te3 nanoparticles with an average size of 32–44 nm were synthesized for the first time on the basis of the natural polysaccharide arabinogalactan and telluride ions generated from elemental tellurium in the system N2H4·H2O–KOH. The phase composition, morphology, and average size of Bi2Te3 nanoparticles were found to be determined by the conditions of their synthesis. Increase of the ratio AG/Bi3+/Te2– is accompanied by reduction of the degree of sphericity and increase of the average size of Bi2Te3 nanoparticles, as well as by the transition of the AG/Bi2Te3 nanocomposite from amorphous to amorphous–crystalline state.

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ACKNOWLEDGMENTS

Experiments were carried out using materials and equipment of Baikal joint analytical center of the Favorsky Irkutsk Institute of Chemistry (Siberian Branch, Russian Academy of Sciences), joint center of the Limnological institute (Siberian Branch, Russian Academy of Sciences), and Isotope-Geochemical Study joint center of the Institute of Geochemistry (Siberian Branch, Russian Academy of Sciences).

Funding

This study was performed in the framework of state assignments to the Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences (project nos. AAAA-A19-119022690046-4, AAAA-A16-116112510011-8).

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Authors and Affiliations

  1. Favorsky Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences, 664033, Irkutsk, Russia

    M. V. Lesnichaya & A. V. Zhmurova

  2. Vinogradov Institute of Geochemistry, Siberian Branch, Russian Academy of Sciences, 664033, Irkutsk, Russia

    A. N. Sapozhnikov

Authors
  1. M. V. Lesnichaya
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  2. A. V. Zhmurova
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  3. A. N. Sapozhnikov
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Correspondence to M. V. Lesnichaya.

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No conflict of interest was declared by the authors.

Additional information

Translated from Zhurnal Obshchei Khimii, 2021, Vol. 91, No. 7, pp. 1120–1129 https://doi.org/10.31857/S0044460X21070167.

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Lesnichaya, M.V., Zhmurova, A.V. & Sapozhnikov, A.N. Synthesis and Characterization of Water-Soluble Arabinogalactan-Stabilized Bismuth Telluride Nanoparticles. Russ J Gen Chem 91, 1379–1386 (2021). https://doi.org/10.1134/S1070363221070161

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