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Synthesis and study of lead(II) uranate Pb(UO2)2O2(OH)2·H2O

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Abstract

An individual crystalline compound Pb(UO2)2O2(OH)2·(H2O) was obtained by reaction of synthetic schoepite UO3·2.25H2O with an aqueous solution of lead(II) nitrate under hydrothermal conditions. The composition and structure of this compound were determined, and the processes of its dehydration and thermal decomposition were studied by chemical analysis, X-ray diffraction, IR spectroscopy, and thermography.

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Authors and Affiliations

  1. Lobachevskii Nizhny Novgorod State University, pr. Gagarina 23a, Nizhny Novgorod, 603950, Russia

    N. G. Chernorukov, O. V. Nipruk, R. V. Abrazheev & K. A. Chaplieva

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  1. N. G. Chernorukov
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  2. O. V. Nipruk
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  3. R. V. Abrazheev
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  4. K. A. Chaplieva
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Corresponding author

Correspondence to O. V. Nipruk.

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Original Russian Text © N.G. Chernorukov, O.V. Nipruk, R.V. Abrazheev, K.A. Chaplieva, 2016, published in Zhurnal Obshchei Khimii, 2016, Vol. 86, No. 9, pp. 1414–1418.

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Chernorukov, N.G., Nipruk, O.V., Abrazheev, R.V. et al. Synthesis and study of lead(II) uranate Pb(UO2)2O2(OH)2·H2O. Russ J Gen Chem 86, 1987–1990 (2016). https://doi.org/10.1134/S1070363216090024

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  • DOI: https://doi.org/10.1134/S1070363216090024

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