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Microwave plasmochemical synthesis of nanopowders in the system Pb-Zr-Ti-O

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Abstract

Conditions for building up the composition and structure of mixed Pb, Zr, and Ti oxides in a microwave plasma-chemical process were studied. As starting substances Pb(C2H5)4, Ti(C4H9O)4, and a 80% Zr(C4H9O)4 solution in 2-propanol were used. To avoid stratification of the components the initial temperature of the flow should not exceed 1000°C. Under these conditions the crystallization of a complex structure requires a combination of a plasma-chemical synthesis with subsequent thermal treatment of the resulting powders. After the thermal treatment an average particle size of lead zirconate-titanate nanopowder was 120 nm.

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Authors and Affiliations

  1. Institute of Chemical Physics Problems, Russian Academy of Sciences, pr. Semenova 18, Chernogolovka, 142432, Russia

    V. I. Torbov, E. N. Kurkin, V. I. Berestenko, I. L. Balikhin, O. D. Torbova, I. A. Domashnev, V. N. Troitskii & S. V. Gurov

Authors
  1. V. I. Torbov
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  2. E. N. Kurkin
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  3. V. I. Berestenko
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  4. I. L. Balikhin
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  5. O. D. Torbova
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  6. I. A. Domashnev
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  7. V. N. Troitskii
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  8. S. V. Gurov
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Corresponding author

Correspondence to E. N. Kurkin.

Additional information

Original Russian Text © V.I. Torbov, E.N. Kurkin, V.I. Berestenko, I.L. Balikhin, O.D. Torbova, I.A. Domashnev, V.N. Troitskii, S.V. Gurov, 2008, published in Zhurnal Obshchei Khimii, 2008, Vol. 78, No. 3, pp. 358–363.

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Torbov, V.I., Kurkin, E.N., Berestenko, V.I. et al. Microwave plasmochemical synthesis of nanopowders in the system Pb-Zr-Ti-O. Russ J Gen Chem 78, 341–346 (2008). https://doi.org/10.1134/S107036320803002X

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  • DOI: https://doi.org/10.1134/S107036320803002X

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