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Synthesis, Characterization, Crystal Structures, and Biological Activity of Nickel(II), Manganese(II) and Cadmium(II) Complexes Derived from 4-Bromo-N'-(1-(Pyridin-2-YL)ethylidene)benzohydrazide

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Abstract

Three nickel(II), manganese(II) and cadmium(II) complexes, [NiL2] (I), [MnL2] (II) and [Cd(HL)2(NO3)]·NO3 (III), derived from 4-bromo-N'-(1-(pyridin-2-yl)ethylidene)benzohydrazide (HL) were prepared and characterized by IR and UV spectra. Structures of the complexes were further confirmed by single crystal X-ray diffraction techniques (CIF files CCDC nos. 1874307 (I), 1874308 (II), and 1874309 (III)). The Ni atom in complex I and the Mn atom in complex II are in octahedral coordination. The Cd atom in complex III is in square antiprism coordination. The nickel complex is effective on the inhibition of Jack bean urease.

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Funding

This work was supported by the Science and Technology Research Project of Hubei Provincial Department of Education (project no. B2018061), the Hubei Provincial University Teaching Team “Environmental Control and Energy Resource Utilization Teaching Team” (project no. 109), and the Environmental Engineering and Science Major Course Teaching Team of Wuhan Textile University (project no. B2018061).

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Authors and Affiliations

  1. School of Environmental Engineering, Wuhan Textile University, 430073, Wuhan, P.R. China

    H. Zhao, X. P. Tan & Q. A. Peng

  2. Engineering Research Center for Clean Production of Textile Dyeing and Printing, Ministry of Education, 430200, Wuhan, P.R. China

    H. Zhao, X. P. Tan & Q. A. Peng

  3. National Local Joint Engineering Laboratory for Advanced Textile Processing and Clean Production, Wuhan Textile University, 430200, Wuhan, P.R. China

    C. Z. Shi, Y. F. Zhao & Y. M. Cui

Authors
  1. H. Zhao
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  2. X. P. Tan
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  3. Q. A. Peng
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  4. C. Z. Shi
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  5. Y. F. Zhao
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  6. Y. M. Cui
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Corresponding authors

Correspondence to Q. A. Peng or Y. M. Cui.

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Zhao, H., Tan, X.P., Peng, Q.A. et al. Synthesis, Characterization, Crystal Structures, and Biological Activity of Nickel(II), Manganese(II) and Cadmium(II) Complexes Derived from 4-Bromo-N'-(1-(Pyridin-2-YL)ethylidene)benzohydrazide. Russ J Coord Chem 47, 58–65 (2021). https://doi.org/10.1134/S107032842011010X

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  • DOI: https://doi.org/10.1134/S107032842011010X

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