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In Situ TEM Study of Phase Transformations in Nonstoichiometric Ni46Mn41In13 Heusler Alloy

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Abstract

This paper presents a study of the metamagnetostructural transition of the martensitic type in the Ni46Mn41In13 alloy with magnetic shape memory and inverse magnetocaloric effect. Differential scanning calorimetry was used to determine the characteristic temperatures of the direct transformation (start at Ms = 253 K, finish at Mf = 164 K) and the reverse transformation (As = 203 K and Af = 236 K, respectively). The characteristic features of the transformation, that is, a decrease in the temperature of the onset of the direct transformation and the presence of a residual austenite phase, and premartensite states, were studied using transmission electron microscopy. The estimated thickness of the material at which the martensitic transformation is suppressed is 50 nm.

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ACKNOWLEDGMENTS

Electron microscopic studies and the preparation of foils for TEM were carried out at the Interdisciplinary Resource Center “Nanotechnology,” Collective Use Center of the Research Park, St. Petersburg State University.

Funding

The study was supported by the Russian Science Foundation (project no. 20-79-10197).

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Authors and Affiliations

  1. Kotelnikov Institute of Radio Engineering and Electronics, Russian Academy of Sciences, 125009, Moscow, Russia

    D. D. Kuznetsov, A. V. Mashirov, V. G. Shavrov & V. V. Koledov

  2. Mikheev Institute of Metal Physics, Ural Branch, Russian Academy of Sciences, 620108, Yekaterinburg, Russia

    E. I. Kuznetsova

  3. Interdisciplinary Resource Center “Nanotechnology,” Research Park, St. Petersburg State University, 199034, St. Petersburg, Russia

    A. S. Loshachenko & D. V. Danilov

  4. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, 119991, Moscow, Russia

    G. A. Shandryuk

Authors
  1. D. D. Kuznetsov
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  2. E. I. Kuznetsova
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  3. A. V. Mashirov
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  4. A. S. Loshachenko
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  5. D. V. Danilov
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  6. G. A. Shandryuk
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  7. V. G. Shavrov
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  8. V. V. Koledov
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Corresponding author

Correspondence to D. D. Kuznetsov.

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The authors declare that they have no conflicts of interest.

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Translated by O. Zhukova

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Kuznetsov, D.D., Kuznetsova, E.I., Mashirov, A.V. et al. In Situ TEM Study of Phase Transformations in Nonstoichiometric Ni46Mn41In13 Heusler Alloy. Phys. Solid State 64, 15–21 (2022). https://doi.org/10.1134/S1063783422010115

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  • DOI: https://doi.org/10.1134/S1063783422010115

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