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Specific features of the formation of vanadium oxide micro- and nanocrystals during gas-phase synthesis

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Abstract

A modified method of gas-phase synthesis of vanadium oxide micro- and nanocrystals was developed. The morphology of the crystals obtained and its dependence on the synthesis conditions are analyzed. The method is shown to permit the growth of rod-shaped crystals rectangular in cross section, whiskers, crystals with a rectangular cavity, and also lamellar crystals and planar ordered textures consisting of oriented rodshaped crystals. The microcrystals synthesized were used to study the mutual reversible transformation of various vanadium oxides using oxidation and reduction reactions.

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Authors and Affiliations

  1. Research-and-Production Corporation Vavilov State Optical Institute, Birzhevaya liniya 12, St. Petersburg, 199034, Russia

    O. P. Vinogradova & A. I. Sidorov

  2. Ioffe Physicotechnical Institute, Russian Academy of Sciences, Politekhnicheskaya ul. 26, St. Petersburg, 194021, Russia

    V. A. Klimov, E. B. Shadrin & A. V. Nashchekin

  3. Herzen State Pedagogical University, nab. Reki Moĭki 48, St. Petersburg, 191186, Russia

    S. D. Khanin & V. Yu. Lyubimov

Authors
  1. O. P. Vinogradova
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  2. A. I. Sidorov
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  3. V. A. Klimov
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  4. E. B. Shadrin
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  5. A. V. Nashchekin
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  6. S. D. Khanin
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  7. V. Yu. Lyubimov
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Correspondence to A. I. Sidorov.

Additional information

Original Russian Text © O.P. Vinogradova, A.I. Sidorov, V.A. Klimov, E.B. Shadrin, A.V. Nashchekin, S.D. Khanin, V.Yu. Lyubimov, 2008, published in Fizika Tverdogo Tela, 2008, Vol. 50, No. 7, pp. 1177–1183.

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Vinogradova, O.P., Sidorov, A.I., Klimov, V.A. et al. Specific features of the formation of vanadium oxide micro- and nanocrystals during gas-phase synthesis. Phys. Solid State 50, 1227–1233 (2008). https://doi.org/10.1134/S1063783408070068

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  • DOI: https://doi.org/10.1134/S1063783408070068

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