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Synthesis, Single Crystal Structure and Characterization of N-Benzylmethylammonium Trifluoromethanesulfonate

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Abstract

The title compound, C9H12NO3F3S, was synthesized and characterized by elemental analyses, IR spectroscopy, thermogravimetric analysis and single crystal X-ray diffraction. The crystals are monoclinic, space group P21/c, Z = 4, The structure is stabilized by N–H···O and C–H···F hydrogen-bonds forming a three-dimensional network.

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ACKNOWLEDGMENTS

We are grateful for financial support from the Science and Technology Project of Jiangxi Provincial Education Department (GJJ171130, GJJ171141), the National Natural Science Foundation of China (Grant no. 51862030, 51563020), Engineering and Technology Research Center for Environmental Protection Materials and Equipment of Jiangxi Province (jxhbclyzb012, jxhbclyzb011) and the Science and Technology Project of Pingxiang Jiangxi Province (ZC201701). We would like to thank the J.H. Luo’s group of Fujian Institute of Research on the Structure of Matter of the Chinese Academy of Sciences for its performance test.

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Authors and Affiliations

  1. Engineering and Technology Research Center for Environmental Protection Materials and Equipment of Jiangxi Province, Pingxiang University, 337055, Pingxiang, Jiangxi, China

    Shi-Geng Li, Guang-Hua He & Bai-Hua Long

  2. Department of Material and Chemistry Engineering, Pingxiang University, 337055, PingXiang, JiangXi, China

    Shi-Geng Li, Guang-Hua He & Bai-Hua Long

  3. School of Electromechanical Engineering, Pingxiang University, 337055, Pingxiang, Jiangxi, China

    Tao-Tao Li

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  1. Shi-Geng Li
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  2. Guang-Hua He
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  3. Tao-Tao Li
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  4. Bai-Hua Long
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Correspondence to Shi-Geng Li or Bai-Hua Long.

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Li, SG., He, GH., Li, TT. et al. Synthesis, Single Crystal Structure and Characterization of N-Benzylmethylammonium Trifluoromethanesulfonate. Crystallogr. Rep. 64, 1062–1065 (2019). https://doi.org/10.1134/S1063774519070083

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  • DOI: https://doi.org/10.1134/S1063774519070083

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