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Liquid membrane potentiometric sensor for determination of Fe3+ ion

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Abstract

Solution studies showed a selective interaction between the new synthesized ionophore, 2-[(thiophen-2-yl)methyleneamino]isoindoline-1,3-dione (TMID) and Fe(III) ion. Therefore, TMID was used as an iron selective ion-carrier in a plasticized liquid membrane sensor. The linear response range of the proposed electrode was 1.0 × 10−6–1.0 × 10−2 M. The Nernstian slope of 20.1 ± 0.3 mV/decade, and a detection limit of 5 × 10−7 M was obtained. The sensor could be used in the pH range of 2.3–4.8, and the response time was about 10 s. The lifetime of the electrode was at least 7 weeks. The sensor accuracy was investigated in two ways: (i) with the potentiometric titration of a Fe3+ solution with EDTA and (ii) with Fe(III) monitoring in some cationic mixtures. Finally, the newly fabricated electrode was effectively applied as an indicator electrode for the direct Fe3+ determination in real samples.

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Authors and Affiliations

  1. Department of Applied Chemistry, Mashhad Branch, Islamic Azad University Mashhad, Mashhad, Iran

    Hassan Ali Zamani & Farnoush Faridbod

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  1. Hassan Ali Zamani
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  2. Farnoush Faridbod
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Correspondence to Hassan Ali Zamani.

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Zamani, H.A., Faridbod, F. Liquid membrane potentiometric sensor for determination of Fe3+ ion. J Anal Chem 69, 1073–1078 (2014). https://doi.org/10.1134/S1061934814110069

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