Abstract
An analysis of olive, pressed sunflower, extracted sunflower, extracted soybean, deodorized sunflower, deodorized rapeseed, and deodorized corn vegetable oils has been performed on an FlavourSpec® ionmobility spectrometer. Twenty-four compounds were found in the spectra of the gas phase above samples of vegetable oils and 12 of them were identified. Ion-mobility spectrometry combined with polycapillary chromatography columns made possible distinguishing oils from different plants, as well as pressed and extracted sunflower oil by the volatile components found in the gas phase above the oil.
Similar content being viewed by others
References
Karachentsev, G.V., Usp. Khim., 1996, vol. 65, no. 8, p. 712.
Eiceman, G.A. and Karpas, Z., Ion Mobility Spectrometry, London: Taylor and Francis, 2005, 2nd Ed.
Berant, Z., Shahal, O., and Karpas, Z., J. Phys. Chem., 1991, vol. 95, p. 7534.
Hill, H.H. and Baim, M.A., Science, 1993, vol. 260, p. 143.
Crawford, C.L., Graf, S., Gonin, M., Fuhrer, K., Zhang, X., and Hill, H.H., Jr., Int. J. Ion Mobil. Spectrom., 2011, vol. 14, p. 23.
Buryakov, I.A. and Kolomiets, Yu.N., J. Anal. Chem., 2003, vol. 58, no. 10, p. 944.
Vautz, W., Zimmermann, D., Hartmann, M., Baumbach, J.I., Nolte, J., and Jung, J., Food Additiv. Contaminant., 2006, vol. 23, p. 1064.
Garrido-Delgado, R., Arce, L., and Valcarcel, M., Anal. Bioanal. Chem., 2012, vol. 402, p. 489.
Ruzsanyi, V., Baumbach, J.I., Sielemann, S., et al., J. Chromatogr. A, 2005, vol. 1084 I, p. 145.
Kornienko, E.A., Mileiko, V.E., Samokish, V.A., and Nazhiganov, O.N., Pediatr., 1999, no. 1, p. 37.
Armenta, S. and Blanco, M., Anal. Chim. Acta, 2011, vol. 703.
Hajialigol, S., Ghorashi, S.A., Alinoori, A.H., Torabpour, A., and Azimi, M., J. Chromatogr. A, 2012, vol. 1268, p. 123.
Buryakov, I.A., Kolomiets, Yu.N., Bolotov, A.V., Vasin, A.I., and Vlasov, Yu.N., J. Anal. Chem., 2002, vol. 57, no. 7, p. 606.
Smolin, Yu.M., Kobtsev, B.N., and Novoselov, N.P., Khim. Khim. Tekhnol., 2009, vol. 52, no. 12, p. 108.
Buryakov, I.A. and Baldin, M.N., J. Anal. Chem., 2008, vol. 63, no. 8, p. 787.
Marquez-Sillero, I., Aguilera-Herrador, E., Cardenas, S., and Valcarcel, M., Trends Anal. Chem., 2011, vol. 30, no. 5, pp. 677.
Buryakov, I.A., J. Anal. Chem., 2011, vol. 66, no. 11, p. 1095.
Kochhar, S.P., Oxidative Pathways to the Formation of Off-Flavours, in: Food Taints and Off-Flavours, Glasgow: Blackie Academic and Professional, 1996, 2nd ed.
Garrido-Delgado, R., Mercader-Trejo, F., Sielemann, S., de Bruyn, W., Arce, L., and Valcarcel, M., Anal. Chim. Acta, 2011, vol. 696, p. 108.
Guillen, M.D. and Cabo, N., J. Agric. Food Chem., 1999, vol. 47, p. 709.
Richards, A., Wijesundera, C., and Salisbury, P., J. Amer. Oil Chem. Soc., 2005, vol. 82, no. 12, p. 869.
Guillen, M.D., Cabo, N., Ibargoitia, M.L., and Ruiz, A., J. Agric. Food Chem., 2005, vol. 53, no. 4, p. 1093.
Frankel, E.N., Neff, W.E., and Selke, E., Lipids, 1981, vol. 16, no. 5, p. 279.
Keszler, A., Kriska, T., and Nemeth, A., J. Agric. Food Chem., 2000, vol. 48.
Sakodynskii, K.I., Brazhnikov, V.V., Volkov, S.A., Zel’venskii, V.Yu., Galkina, E.S., and Shatts, V.D., Analiticheskaya khromatografiya (Analytical Chromatography), Moscow: Khimiya, 1993.
Dlugogorski, B.Z., Kennedy, E.M., and Mackie, J.C., Ind. Eng. Chem. Res., 2012, vol. 51, p. 5645.
Author information
Authors and Affiliations
Additional information
Original Russian Text © E.V. Krisilova, A.M. Levina, V.A. Makarenko, 2014, published in Zhurnal Analiticheskoi Khimii, 2014, Vol. 69, No. 4, pp. 414–420.
Rights and permissions
About this article
Cite this article
Krisilova, E.V., Levina, A.M. & Makarenko, V.A. Determination of the volatile compounds of vegetable oils using an ion-mobility spectrometer. J Anal Chem 69, 371–376 (2014). https://doi.org/10.1134/S1061934814020075
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S1061934814020075