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Separation of four bioactive compounds from Herba artemisiae scopariae by HPLC with ionic liquid-based silica column

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Abstract

Commercial silica was modified with an amino-imidazolium ionic liquid and the obtained particles were used as a special sorbent in HPLC column to separate chlorogenic acid, caffeic acid, scoparone and rutin from Herba artemisiae scopariae. Acetonitrile/water (50 : 50, v/v) and acetonitrile/water (50 : 50, v/v, containing 0.1% triethylamine) mixtures were used as mobile phases for two-stage elutions. Good linearity were obtained from 0.2 × 10−4 to 0.1 mg/mL (r 2 > 0.998) with the relative standard deviations less than 5.2%.

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Authors and Affiliations

  1. Department of Chemical Engineering, Inha University, Incheon, 402-751, Korea

    M. Tian & K. H. Row

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  1. M. Tian
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  2. K. H. Row
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Tian, M., Row, K.H. Separation of four bioactive compounds from Herba artemisiae scopariae by HPLC with ionic liquid-based silica column. J Anal Chem 66, 580–585 (2011). https://doi.org/10.1134/S1061934811060207

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  • DOI: https://doi.org/10.1134/S1061934811060207

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