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Morphology and Structure of a Fine-Grained Composite Material Based on Boehmite Extracted from Aqueous Solutions of Na-Carboxymethyl Cellulose with Aluminum Powder

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Abstract

Fine-grained composite material is synthesized from aluminum powder in aqueous solutions of Na-sodium carboxymethyl cellulose. The phase composition of the composite material is determined using X-ray phase analysis and infrared spectroscopy. Aluminum oxyhydroxide (boehmite) stabilized by the polymer material Na-sodium carboxymethyl cellulose is found to be formed during synthesis. The interaction between boehmite and the polymer material is implemented due to intermolecular hydrogen bonds. The formation of 600-nm spherical particles with porous surfaces is revealed by scanning electron microscopy. Unlike traditional methods of producing boehmite at 200–400°С, synthesis occurs at 70–80°С. The prospects of using boehmite for the creation of porous functional materials are shown.

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Authors and Affiliations

  1. Kamensky Institute, Platov South-Russian State Polytechnic University, Kamensk-Shakhtinsky, Rostov oblast, 346800, Russia

    N. M. Antonova & F. M. Boldyrev

  2. Don State Technical University, Rostov-on-Don, 344000, Russia

    I. Y. Zabiyaka

Authors
  1. N. M. Antonova
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  2. F. M. Boldyrev
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  3. I. Y. Zabiyaka
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Correspondence to N. M. Antonova.

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Original Russian Text © N.M. Antonova, F.M. Boldyrev, I.Y. Zabiyaka, 2018, published in Poverkhnost’, 2018, No. 10, pp. 37–44.

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Antonova, N.M., Boldyrev, F.M. & Zabiyaka, I.Y. Morphology and Structure of a Fine-Grained Composite Material Based on Boehmite Extracted from Aqueous Solutions of Na-Carboxymethyl Cellulose with Aluminum Powder. J. Surf. Investig. 12, 974–981 (2018). https://doi.org/10.1134/S102745101805021X

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  • DOI: https://doi.org/10.1134/S102745101805021X

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