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Use of thin-layer chromatography with closed sorption layer for the determination of volatile compound

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Abstract

For decades, it has been believed in Russian and foreign scientific and technical literature that conventional thin-layer chromatography (TLC) cannot be used for the determination of volatile compounds. Experiments have shown that the version of TLC with a closed adsorbent layer proposed recently at the Topchiev Institute, Russian Academy of Sciences, is applicable to the investigation of the group content of aromatic hydrocarbons in gasoline. It has been found that the best resolution of analyte groups of compounds can be achieved by means of circular chromatography and sample introduction into a chromatographic system, using the frontal variant of chromatography.

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Authors and Affiliations

  1. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Leninskii pr. 29, Moscow, 119991, Russia

    V. G. Berezkin, I. I. Ashrapova, A. V. Chausov, A. S. Lermontov & V. F. Tret’yakov

  2. Lomonosov State Academy of Fine Chemical Technology, pr. Vernadskogo 86, Moscow, 117571, Russia

    E. V. Egorova

  3. All-Russia Research Institute of Oil Processing, Moscow, Russia

    S. A. Leont’eva

Authors
  1. V. G. Berezkin
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  2. I. I. Ashrapova
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  3. A. V. Chausov
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  4. A. S. Lermontov
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  5. V. F. Tret’yakov
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  6. E. V. Egorova
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  7. S. A. Leont’eva
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Corresponding author

Correspondence to V. G. Berezkin.

Additional information

Original Russian Text © V.G. Berezkin, I.I. Ashrapova, A.V. Chausov, A.S. Lermontov, V.F. Tret’yakov, E.V. Egorova, S.A. Leont’eva, 2009, published in Neftekhimiya, 2009, Vol. 49, No. 5, pp. 421–425.

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Berezkin, V.G., Ashrapova, I.I., Chausov, A.V. et al. Use of thin-layer chromatography with closed sorption layer for the determination of volatile compound. Pet. Chem. 49, 401–405 (2009). https://doi.org/10.1134/S0965544109050120

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  • DOI: https://doi.org/10.1134/S0965544109050120

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