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MoO3 − δ nanorods

  • Synthesis and Properties of Inorganic Compounds
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Abstract

Oxygen-deficient molybdenum trioxide nanorods of composition MoO2.987 (orthorhombic, a = 3.951(2) Å, b = 13.856(1) Å, c = 3.700(1) Å) were synthesized by a hydrothermal process (150–180°C, 30–50 h). MoO3 − δ particles were 60–90 nm in diameter; their lengths were several micrometers. X-ray photoelectron and IR spectra of these nanorods were studied, The nanorods had weak paramagnetism, signifying the existence of molybdenum(V) ions in their structure.

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References

  1. X. M. Huang, J. L. Liu, J. L. Chen, et al., Catal. Lett. 108(1–2), 79 (2006).

    Article  CAS  Google Scholar 

  2. T. He and J. N. Yao, J. Photochem. Photobiol. C. 4(2), 125 (2003).

    Article  CAS  Google Scholar 

  3. R. Sivakumar, C. S. Gopinath, M. Jayachandran, and C. Sanjeeviraja, Curr. Appl. Phys. 7(1), 76 (2007).

    Article  Google Scholar 

  4. W. Li, F. Cheng, Z. Tao, and J. Chen, J. Phys. Chem. B 110(1), 119 (2006).

    Article  CAS  Google Scholar 

  5. Y. B. Li, Y. Bando, D. Golberg, and K. Kurashima, Appl. Phys. Lett. 81(26), 5048 (2002).

    Article  CAS  Google Scholar 

  6. A. M. Taurino, A. Forleo, L. Francioso, et al., Appl. Phys. Lett. 88(15), 152111 (2006).

  7. E. Comini, L. Yubao, Y. Brando, and G. Sberveglieri, Chem. Phys. Lett. 407(4–6), 368 (2005).

    Article  CAS  Google Scholar 

  8. G. R. Patzke, F. Krumeich, and R. Nesper, Angew. Chem., Int. Ed. Engl. 41(14), 2446 (2002).

    Article  CAS  Google Scholar 

  9. M. Niederberger, F. Krumeich, H.-J. Muhr, et al., J. Mater. Chem. 11(7), 1941 (2001).

    Article  CAS  Google Scholar 

  10. G. A. Camacho-Bragado and M. Jose-Yacaman, Appl. Phys. A: Mater. Sci. Proc. 82(1), 19 (2006).

    Article  CAS  Google Scholar 

  11. S. Wang, Y. Zhang, X. Ma, et al., Solid State Commun. 136(5), 283 (2005).

    Article  CAS  Google Scholar 

  12. L. Seguin, M. Figlarz, R. Cavagnat, and J.-C. Lassegues, Spectrochim. Acta A 51(8), 1323 (1995).

    Article  Google Scholar 

  13. Intyre N. S. Mc, D. D. Johnston, L. L. Coatsworth, et al., Surf. Interface Anal. 15(2), 265 (1990).

    Article  Google Scholar 

  14. L. A. Bursill, Proc. R. Soc. London, Ser. A 311(7), 267 (1969).

    CAS  Google Scholar 

  15. D. H. Brown and P. G. Perkins, Inorg. Chim. Acta 8, 285 (1974).

    Article  CAS  Google Scholar 

  16. V. I. E. Bruyere, L. A. G. Rodenas, P. J. Morando, and M. A. Blesa, J. Chem. Soc., Dalton Trans., No. 24, 3593 (2001).

  17. N. J. Campbell, A. C. Dengel, C. J. Edwards, and W. P. Griffith, J. Chem. Soc., Dalton Trans., No. 6, 1203 (1989).

  18. W. Dong and B. Dunn, J. Mater. Chem. 8(3), 665 (1998).

    Article  CAS  Google Scholar 

Download references

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Authors and Affiliations

  1. Institute of Solid State Chemistry, Ural Division, Russian Academy of Sciences, ul. Pervomaiskaya 91, Yekaterinburg, 620219, Russia

    V. L. Volkov, G. S. Zakharova & M. V. Kuznetsov

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  1. V. L. Volkov
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  2. G. S. Zakharova
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  3. M. V. Kuznetsov
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Additional information

Original Russian Text © V.L. Volkov, G.S. Zakharova, M.V. Kuznetsov, 2008, published in Zhurnal Neorganicheskoi Khimii, 2008, Vol. 53, No. 11, pp. 1807–1811.

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Volkov, V.L., Zakharova, G.S. & Kuznetsov, M.V. MoO3 − δ nanorods. Russ. J. Inorg. Chem. 53, 1686–1690 (2008). https://doi.org/10.1134/S003602360811003X

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  • DOI: https://doi.org/10.1134/S003602360811003X

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